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Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7714-1 <br /> Client Sample ID: EW1-3' <br /> Lab Sample ID: -720-7714-2 Date Sampled: 02/12/2007 1405 <br /> Client Matrix: Solid Date Received: 02/12/2007 1720 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch:720-18250 Instrument ID: Varian 3900A <br /> Preparation: 5030B Prep Batch: 720-18249 Lab File ID: c:\saturnws\data\200702\02 <br /> Dilution: 200 Initial Weight/Volume: 5.04 g <br /> Date Analyzed: 02/14/2007 0215 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/13/2007 0945 . <br /> ' <br /> Analyte DryWt.Corrected: N Result(mg/Kg) Qualifier R_L_ <br /> Benzene _�.___...�...... ND ......_._....� 0.99µ____.-.._,..._....., <br /> Ethylbenzene ND 0.99 <br /> Toluene ND 0.99 <br /> MTBE ND 0.99 <br /> Xylenes,Total ND 2.0 <br /> Gasoline Range Organics(GRO)-C5-C12 500 50 <br /> Surrogate _ %Rec Acceptance Limits <br /> Toluene-d8(Burr)�..._a..�.._._...._,__�.._..._.._.._ w�._. ,�.__...�.�89�....��...�....�_e._.� �. ,50-130 <br /> 1,2-Dichloroethane-d4(Surr) 101 60-140 <br /> I <br /> �f <br /> STL San Francisco Page 8 of 21 <br />