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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ihttp//wwwmc2gMabelIcorn E-mail main@mccampbell cam <br /> IAdvanced GeoEnvironmental Client Project M Larrys Auto Date Sampled 06/08/01 <br /> 837 Shaw Road Date Received 06/13/01 <br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 06115-06119/01 <br /> Client P O Date Analyzed 06/15-06/19/01 <br /> I Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab 1D 69662 <br /> Client ID MW7/060801 <br /> Matrix W <br /> Repotting IamU Reβ€”.9 tame <br /> Compound Concentration* W S Compound Concentration* W S <br />' Acetone 1 ND 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene 23 to 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 50 <br />' Bromochloromethanc ND 10 5 0 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 5 0 <br />' n-Butyl benzene ND to 50 Methyl butyl ketones ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride') ND 10 5 0 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone I ND 10 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) --- 10 5 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 50 <br /> Chloroethane ND 10 50 n-Propyl benzene i 1 10 1 5 0 <br /> 2-Chioroethyl Vinyl Ethe ND 10 50 Styrene ND 1 0 5 0 <br />' Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2β€ž2-Tetrach]oroettrane ND 10 50 <br /> 2-ChlorotolueneND 10 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 10 5 0 Toluene ND 1 0 50 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,44nchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 10 E5 0 1,1,2-Tnchloroethane ND 10 50 <br />' 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 10 50 Tnchlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 10 5 0 <br /> 1,1-134chloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br />' l,2-Dichloroethane ND 10 50 1,3,54nmethylbenzenc ND 105 0 <br /> IND D 1 0 50 Vinyl Acetate ImJ ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chlonde a ND 10 50 <br /> trans-1,2-Dichloroethene ND 10 5 0 Xylenes,total ND I O 50 <br />' 12-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 106 <br /> ],l-Dichloropropene ND 10 5 0 Toluene-d8 100 <br />' cis-1,3-Dichloropropene ND 10 5 0 4-13romofluorobenzene 100 <br /> 'water and vapor samples are reported in ugIL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethenc-, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than β€”5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(a)dimethylbenzenes <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />