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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//wwwrnc2Mpbcllcorn E-mail main@mccampbell cam <br />' Advanced GeoEnvironmental Client Project ID Larrys Auto Date Sampled 06/08/01 <br /> 837 Shaw Road Date Received 06/13/01 <br />' Stockton, CA 95215 Client Contact Calvm Lee Date Extracted 06115-06/19101 <br /> Client P O Date Analyzed 06/15-06/19101 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 69663 <br />' Client 1D VW2B/060801 <br /> Matrix .mW <br /> Reporting Lut * Repor"g Lormt <br /> Compound Concentration" W S Compound Concentration W S <br />' Acetone W ND<1800 50 25 trans-l,3-Dichloropropene ND<1000 1 0 5 0 <br /> Benzene 45,000 10 5 0 Ethylene dibrortude ND<1000 1 0 5 0 <br /> Bromobenzene ND11000 1 0 5 0 Ethylbenzene 2900 1 0 5 0 <br />' Bromochloromethane ND<1000 1 0 5 0 Hexachlorobutadiene ND<1000 5 0 25 <br /> Bromodichloromethane ND<1000 1 0 5 0rn-Propyl <br /> methane ND<1000 1 0 5 0 <br /> Bromoform ND<1000 10 5 0mpylbenzene ND<1000 1 0 50 <br /> Bromomethane ND<1000 10 5 0 opropyl toluene ND<1000 10 50 <br />' n-Butyl benzene ND<1000 1 0 5 0yl butyl ketone ND<1000 1 0 so <br /> sec-Butyl benzene ND<1000 1 0 5 0ylene Chlonde` ND<1500 l 0 50 <br /> tent-Butyl benzene ND<1000 1 0 5 0yl ethyl ketone ND<1000 2 0 10 <br /> Carbon Disulfide ND<1000 1 0 5 0thyl rsobutyl ketone g ND<1000 1 0 5 0 <br /> Carbon Tetrachloride ND<1000 1 0 5 0thyl tert-Butyl Ether(MTBE) -- 1 0 50 <br /> Chlorobenzene ND<1400 1 0 S ahthalene ND<1000 5 0 50 <br /> Chloroethane ND<1000 1 0 5 0ropyl benzeneND<1OOD 1 0 50 <br /> 2-Chlomethyl Vinyl Ether` ND<1000 1 0 5 0rene ND<1000 1 0 5 0 <br /> Chloroform ND<1000 10 50 ,1,2-Tetrachloroethane ND<1000 10 50 <br /> Chloromethane NIK1000 10 5 0 ,2,2-Tetrachloroethane ND<1000 14 50 <br /> 2-Chlorotoluene ND<1000 10 5 0rachloroethene ND<1000 10 50 <br /> 4-Chlorotoluene ND<1000 10 5 0uene34,000 10 50 <br /> Dibromochioromethane ND<1000 10 50 ,3-Tnchlorobenzene ND<1000 5 0 25 <br /> 1,2-13ibrorno-3-chloropropane ND<1000 2 0 10 1,2,4-Trichlorobenzene ND<1000 5 0 25 <br /> Dibromomethane ND<1000 10 50 1,1,1-Tnchloroethane ND<1000 10 50 <br /> 1,2-Dichlorobenzene ND<1000 10 50 1,1,2-Tncbloroethane ND-,1000 10 50 <br />' 1,3-Dichlorobenzene ND<1000 1 0 5 0 Trichloroethene ND<1000 1 0 50 <br /> 1,4-Dichlorobenzene ND<1000 1 0 5 0 Tnchlorofluorometharte ND<1000 1 0 50 <br /> Dichlorodifluoromethane ND<1000 1 0 5 0 1,2,3-Tnchloropmpane ND<1000 10 50 <br /> 1,1-Dichloroethane ND<1000 10 50 1,2,4-Tnmethylbenzene 1600 10 50 <br />' 1,2-Dichloroethane 1400 ] 0 5 0 1,3,5-Tnmethylbenzene ND<1000 10 50 <br /> 1,1-Dichloroethene ND<1000 1 0 5 0 Vinyl Acetate m ND<1000 5 0 25 <br /> cis-1,2-Ihchloroethene ND<1000 1 0 5 0 Vinyl Chloride ° ND<1000 1 0 5 0 <br /> trans-1,2-Dichloroethene ND<1000 1 0 5 0 Xylenes,total 15,000 1 0 50 <br /> 1,2-Dichioropropane ND<1000 1 0 1 5 0 Comments <br /> 1,3-Dichloropropane ND<1000 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<1000 l 0 5 0 Dibromol]uoromethane 98 <br /> 1,1-1>ichloropropene ND<1000 1 0 5 0 Toluene-d8 106 <br />' cis-1,3-Dichloropropene ND<1000 1 0 5 0 4-Bromofluorobenzene 108 <br /> 'water and vapor samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br />' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropyiacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (I) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 SA— <br /> Edward Hamilton,Lab Director <br /> 1 <br />