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I110 2nd Avenue South,##D7,Pacheco,CA 94553-5560
<br /> ® McCA DBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br />' linp//www mccamybell coat E-mail mam@mccampbell corn
<br />' Advanced GeoEnvironmental Client Protect ID Larrys Auto Date Sampled 06/08/01
<br /> 837 Shaw Road Date Received 06/13/01
<br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 06/15-06/19/01
<br /> Client P O Date Analyzed 06/15-06/19/01
<br />' Volatile Organics By GC/MS
<br /> EPA method 8264
<br /> Lab ID 69666
<br /> t Client ID VW513/060801
<br /> Matrix W
<br /> Reporting Lvntt Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W 5
<br />' Acetone ro NIX1000 50 25 trans-1,3-Dichloropropene ND<500 10 50
<br /> Benzene 4500 1 0 5 0 Ethylene dibromide ND<500 10 5 0
<br /> Bromobenzene ND<500
<br /> _F07 5 0 Ethylbenzene 4800 10 5 0
<br />' Bromochloromethane ND<500 10 5 0 Hexachlorobutadiene ND<500 50 25
<br /> Bromodichloromethane ND<500 10 5 0 lodomethane ND<500 1 0 5 0
<br /> Bromoform ND<500 1 0 5 0 Isopropylbenzene NIX500 10 5 0
<br /> Bromomethane ND<500 10 50 p-Isopropyl toluene ND<500 to- 50
<br /> n-Butyl benzcnc ND<500 10 50 Methyl butyl ketone ND<500 10 5 0
<br />' sec-Butyl benzene ND<500 1 0 50 Methylene Chloride"' ND<750 10 5 0
<br /> ter(-Butyl benzene ND<500 1 0 50 Mcthyl ethyl ketone ND<500 2 0 10
<br /> Carbon Disulfide ND<500 1 0 50 Methyl isobutyl ketone ND<500 1 0 50
<br /> Carbon Tetrachloride N13<500 10 50 Methyl tert-Butyl Ether(MTBE) --- 10 5 0
<br /> Chlorobenzene ND<500 10 50 Naphthalene ND<500 5 0 50
<br /> Chloroethane ND<500 10 5 0 n-Propyl benzene ND<500 10 50
<br /> 2-Chloroethyl Vinyl Eth ND<500 1 0 50 Styrene ND<500 10 5 0
<br /> Chloroform ND<500 10 50 1,1,1,2-Tetrachloroethane ND<500 10 50
<br /> Chloromethane ND<500 1 0 50 1,1,2,2-Tetrachloroethane ND<500 10 5 0
<br /> 2-Chlorotoluene ND<500 1 0 50 Tetrachloroethene ND<500 to 50
<br /> 4-Chlorotoluene ND<500 1 0 5 0 Toluene 36,000 10 50
<br /> Dibromochloromethane ND<500 1 0 50 1,2,3-Tnchlorobenzene ND<500 50 25
<br /> 1,2-Dibromo-3-chloropropane N13<500 20 10 1,2,4-Trichlorobenzcne ND<500 5 0 25
<br /> Dibromomethane ND<500 1 0 so 1,1,1-Tnchloroethane ND<500 10 50
<br /> 1,2-Dichlorobenzene ND<500 10 50 1,1,2-Tnchloroethane ND<500 10 5 0
<br />' 1,3-Dichiorobenzene ND<500 10 50 Trichloroethene ND<500 10 5 0
<br /> 1,4-Dichlorobenzene ND<500 10 5 0 Tnchlorofluoromethane ND<500 10 50
<br /> Dichlorodifluoromethane ND<500 1 0 5 0 1,2,3-Tnchloropropane NIX500 1 05 0
<br /> M-Dichloroethane ND<500 10 50 1,2,4-Trimethylbenzene 3200 10 50
<br />' 1,2-Dichloroethane ND<500 10 50 1,3,5-Tnmethylbenzene 820 1 0 50
<br /> ],I-Dichloroethene ND<500 10 50 Vinyl Acetate '° ND<500 LLLO 5
<br /> cis-1 2-Dichloroethene ND<500 1 0 50 Vinyl Chloride ND<500
<br /> trans-1,2-Dichloroethene ND<500 1 0 50 Xylenes,total 25,00(1
<br />' 1,2-Dichloropropane NIX500 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND<500 1 0 5 0 Surrogate Recoveries{%)
<br /> 2,2-Dichloropropane ND<500 I 1 0 M 5 0 Dibromofluoromethane 96
<br /> 1,1-Dichloropropene ND<500 1 0 1 50 Toluene-d8 106
<br /> cis-1,3-Dichloropropene ND<500 10 5 0 4-Bromofluarobenzene 108
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br />' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br />' DHS Certification No 1644 Edward Hamilton,Lab Director
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