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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> ® McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' hn I/www mccamubcll com E-mail team@mccampbell com <br />' Advanced GeoEnvlronmental Client Project ID Larrys Auto Date Sampled 06/08/01 <br /> 837 Shaw Road Date Received 06/13/01 <br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 06/15-06/19/01 <br /> Client P O Date Analyzed 06/15-06/19/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 69665 <br /> t Client 1D VW4/060801 <br /> Matrix W <br /> Reporting Lams! Reporting L irmt <br /> Compound Concentration* W S Compound Concentration* W S <br />' Acetone ro) ND<250 50 25 trans-1,3-Dichloropropene ND<130 1 0 50 <br /> Benzene 10,000 10 50 Ethylene dibromde ND<130 1 0 50 <br /> Bromobenzene ND<130 10 50 Ethylbenzene 2400 i 0 5 0 <br />' Bromochlaromethane ND<130 10 50 Hexachlorobutadicne ND<130 50 25 <br /> Bromodichloromethane ND<130 10 50 lodomethane ND<130 10 so <br /> Bromoform ND<130 10 50 Isopropylbenzene ND<130 10 50 <br /> Bromomethane ND<130 10 50 p4sopropyl toluene ND<130 10 50 <br /> n-Butyl benzene ND<130 10 50 Methyl butyl ketone ND<130 10 50 <br /> sec-Butyl benzene ND<130 10 50 Methylene ChloridePT ND<190 10 50 <br /> tert-Butyl benzene ND<130 1 0 50 Methyl ethyl ketone ND<130 —T-0— 10 <br /> Carbon Disulfide ND<130 10 50 Methyl isobutyl ketone ND<130 1 0 50 <br /> Carbon Tetrachloride ND<130 10 50 Methyl tert-Butyl Ether(MTBE) 10 50 <br /> ChloTobenzene ND<130 1 0 50 Naphthalene 930 50 50 <br /> Chloroethane ND<130 10 50 n-Propyl benzene 1 220 10 50 <br /> 2-Chlormthyl Vinyl Ether"' ND<130 10 50 Styrene7T ND<130 10 50 <br />' Chloroform ND<130 1 0 50 1,1,1,2-Tetrachloroethane ND<130 to 50 <br /> Chloromethane ND<130 1 0 50 1,1,2,2-Tetrachloroethane ND<130 10 5 0 <br /> 2-Chlorotoluene ND<130 1 0 50 Tetrachloroethene ND<130 10 50 <br /> 4-Chlorotoluene ND<130 1 0 50 Toluene 4300 10 50 <br />' Dtbromochloromethane ND<130 10 50 1,2,3-Tnchlorobenzene ND<130 50 25 <br /> 1,2-Dibromo-3-chloropropane ND<130 20 10 1,2,4-Trichlombenzene ND<130 5 0 25 <br /> Dibromomethane ND<130 10 50 1,1,1-Tnchloroethane ND<130 10 50 <br /> 1,2-Dichlorobenzene ND<130 10 50 1,1,2-Tnchloroethane ND<130 10 5 0 <br />' 1,3-Dichlorobenzene ND<130 1 0 5 0 Trichloroethene ND<130 1 0 50 <br /> 1,4-Dichlorobenzene ND<130 10 5 0 Tncblorofluoromethane ND<130 10 50 <br /> Dichlorodifluoromethane ND<130 10 5 0 1,2,3-Tnchlorupropane ND<130 10 5 0 <br /> 1,1-Dichlotoethane ND<130 1 0 50 1,2,4-Tnrnethylbenzene 2400 10 50 <br /> t 1,2-Dichloroethane ND<130 10 50 i,3,5-Tnmethyibenzene 630 10 5 0 <br /> 1,1-Dichloroethene ND<130 1 0 50 Vinyl Acetate m ND<130 50 25 <br /> cis-1,2-Dichlormthene NIK130 10 5 0 Vinyl Chloride " ND<130 10 50 <br /> trans-1,2-Dichlomethene N13<130 1 0 50 Xylenes,total 7700 10 50 <br /> 1,2-Dichioropropane ND<130 10a5O <br /> EDibTomofluoromethane <br /> s <br /> 1,3-Dichloropropane ND<130 1 0Surrogate Recoveries <br /> 2,2-Dichloropropane ND<130 10 101 <br /> 1,1-Dichloropropene ND<130 1 08 107 <br /> cis-1,3-1hchloropropene ND<130 10uorobenzene 108 <br /> 'water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />' (b) 2 proparione or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water uniniscrble sheen is present, (i)liquid sample that contains greater than -4 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (I) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />