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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' hap://www,mcQampbell com E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Protect ID Larry's Auto Repair Date Sampled 11/22/99 <br /> 4005 North Wilson Way Date Received 11/23/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 11123-11/30199 <br /> Client P O Date Analyzed 11/23-11/30/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 26114 <br />' Client ID MW-3111-22-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone mi ND trans-1,3-Dtchloropropene ND <br /> Benzene 21 Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene 4 7 <br /> BTOMOchloromethane ND Hexachlorobutadiene ND <br />' Bromodichloromethane ND lodomethane ND <br /> BTOmofonn ND Isopropylbenzene 1 ] <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br />' sec-Butyl benzene ND Methylene Chlonde" ND <br /> terf-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide NO Methyl isobutyl ketone a ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene 21 <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether` ND Styrene ND <br /> Chloroform 3 0 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene m 12 <br /> Dibromochloromethane ND 1,2,3 Tncblorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchi0robenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnchloroethane ND <br />' 1,3-Dichlorobenzene ND TnchlOToethene ND <br /> 1,4-Dichlorobenzene ND TnchlorofluorOmethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> l,]-Dichloroethane ND 1,2,4-Tnmethylbenzene 3 8 <br />' 1,2-Dichloroethane 1 4 1,3,5-Tnmethylbenzene 1 2 <br /> 1,1-Dichloroethene ND Vinyl Acetate'") ND <br /> cis 1,2-Dichloroethene ND Vinyl Chloride ND <br /> t7ans-1,2-Dichloroethene ND Xylenes,total 21 <br />' 1,2-Dichloropropane ND Comments <br /> 1,3-DichlOropropane ND Surrogate Recouries(%) <br /> 2,2-Dichloropropane ND DlbromoflUOrOmethane 96 <br /> 1,]-Dichloropropene ND Toluene-d8 100 <br />' cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 93 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than ---5 vol % <br /> sediment, G) sample diluted due to high organic content, (k) ethenyibenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1b44 Edward Hamilton, Lab Director <br />