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' I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htWL/w_wwmcc=pbgL1_wm E-mail main@mccampbell corn <br /> i <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Repair Date Sampled 11/22/99 <br /> 4005 North Wilson Way Date Received 11/23/99 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/23-11/29/99 <br /> Client P O Date Analyzed 11/23-11/29/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 26115 <br />' Client ID MW-4/11-22-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone rn> ND<1100 trans-1,3-Dichloropropene ND<500 <br /> Benzene 21,000 Ethylene dibromide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 2400 <br /> Bromochloromethane ND<500 Hexachlorobutadiene ND<500 <br />' Bromodichloromethane ND<500 lodomethane ND<500 <br /> Bromoform ND<500 lsopropylbenzene ND<500 <br /> Bromomethane ND<500 p-Isopropyl toluene ND<500 <br /> n-Butyl benzene ND<500 Methyl butyl ketone ND<500 <br /> t sec-Butyl benzene ND<500 Methylene Chloride") ND<690 <br /> tert-Butyl benzeneND<500 Methyl ethyl ketone 1200 <br /> Carbon Disulfide ND<500 Methyl isobutyl ketone ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<500 Naphthalene 1400 <br /> Chloroethane ND<500 n-Propyl benzene ND<500 <br /> 2-Chloroethyl Vinyl Ether"I ND<500 Styrene ND<500 <br /> Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500 <br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500 <br /> 2-Chlorotoluene ND<500 Tetrachloroethene ND<550 <br /> 4-Chlorotoluene ND<500 Toluenem) 16,000 <br /> Dibromochloromethane NLX500 1,2 3-Tnchlorobenzene ND<500 <br />' 1,2-Dibromo-3-chloropropane ND<500 1,2,4-Trichlorobenzene ND<500 <br /> Dibromomethane ND<500 1,1,1-Trichloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Tnchl oroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Trichloroethene ND<500 <br /> 1,4-Dichlorobenzene ND<500 Tnchlorofluoromethane ND<500 <br /> Dichlorodifluoromethane ND<500 1,2,3-Trichloropropane ND<500 <br /> ],1-Dichloroethane ND<500 1,2,4-Tnme1hylbenzene 1700 <br /> 1,2-Dichloroethane 690 l,3,5-Tnmethy]benzene ND<500 <br />' 1,1-Dichloroethene ND<500 Vinyl Acetate ° ND<500 <br /> cis-1,2-Dichlorocthene ND<500 Vinyl Chloride ° ND<500 <br /> trans-1,2-Dichloroethene NIX500 Xylenes,total 13,000 <br />' 1,2-Dichloropropane ND<500 Comments <br /> 1,3-Dichloropropane ND<500 Surrogate Reco%cries(%) <br /> 2,2-Dichloropropane NTX500 Dibromofluoromethane 96 <br /> 1,1-Dichloropropene ND<500 Toluene-d8 44 <br />' cis-1,3-Dichloropropene ND<500 I 4-BromofluoTobenzene 91 <br /> Rater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,tripes in ug/wr)pe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated Aater samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 Zug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (1) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />