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I <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h I/www mcg, Ecom E-mail rnatn@mccampbell cont <br />' Date Sampled 11/22/99 <br /> Advanced GeoEnvironmental Client Protect ID Larry's Auto Repair <br /> Date Received 11/23/99 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11123-11130199 <br /> Client P 0 Date Analyzed 11/23-11130199 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 26120 <br />' Client ID VW-513/11-22-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone m ND<12,000 trans-1,3-Dichloropropene ND<1000 <br /> Benzene 13,000 Ethylene dibromide NLK1000 <br /> Bromobenzene ND<1000 Ethylbenzene 7200 <br /> Bromochloromethane ND<1000 Hexachlorobutadiene ND<1000 <br /> t Bromodichloromethane ND<1000 lodomethane ND<1000 <br /> Bromafotm ND<I 000 Isopropylbenzene ND<1000 <br /> Bromomethane ND<1000 p-Isopropyl toluene NDc1000 <br /> n Butyl benzene ND<l000 Methyl butyl ketone` ND<1000 <br />' ND<6300 <br /> sec-Butyl benzene ND<1000 Methylene Chloride"; <br /> ten-Butyl benzene ND<1 000 Methyl ethyl ketone 1100 <br /> Carbon Disulfide ND<1000 Methyl isobutyl ketones WND<1000 <br /> Carbon Tetrachloride ND<1000 Methyl tert-Butyl Ether(MTBE) <br /> Chlorobenzene ND<1000 Naphthalene <br /> Chloroethane ND<1000 n-Propyl benzene <br /> 2-Chloroethyl Vinyl Ether` NIK1000 Styrene <br /> Chi oroform N IK 1000 1,1,1,2-Tetrachl oroethane N D<1000 <br /> Chloromethane ND<l 000 1,1,2,2-Tetrachloroethane ND<1000 <br /> 2-Chlorotoluene ND<1000 Tetrachloroethene ND<1800 <br /> 4-Chlorotoluene ND<1000 Toluene m 56,000 <br /> Dibromochloromethane ND<1000 1,2,3-Tnchiorobenzene ND<1000 <br /> 1,2-Dibromo-3-chloropropane ___9r)<1000 1,2,4-Tnchlorobenzene ND<IODO <br /> Dibrotiiometharie ND<1000 1,1,1-Trichloroethane ND<1000 <br /> 1,2-Dichlorobenzene ND<I 000 1,1,2-Trichloroethane ND<1000 <br /> 1,3-Dichlorobenzene ND<1000 Tnchioroethene ND<1000 <br />' 1,4-Dichlorobenzene ND<1000 Tnchlorofluoromethane ND<1000 <br /> Dichlorodifiuoromethan e ND<1000 1,2,3-Tnchioropropane N I3�1000 <br /> 1,I-Dichloroethane N D<1000 1,2,4-Tnmethylbenzene 3900 <br /> 1,2-Dichloroethane ND<1000 1,3,5-Tnmethylbenzene 1000 <br /> 1,1-Dichloroethene 95<1000 Vinyl Acetate ° ND<1000 <br /> cis-1,2-Dichloroethene ND<]000 Vinyl Chloride ° N1K1000 <br /> trans-1,2-Dichloroethene ND<]000 Xylenes,total 3],000 <br /> 1,2-Di chloropropane ND<1000 Comments <br /> 1,3-Dichloroprvpane <br /> ND<1000 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<1000 DibromoZramethane 97 <br /> 1,1-Dichloropropene ND<1000 Toluene- 102 <br /> cis-1,3Dwhioroprapene ND<1000 4-Brmorobenzene 87 <br /> mater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,Wipes in ug/vatpe and,ill TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-prop2none or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2 hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen is present, (1) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> Edward Hamilton,Lab Director <br /> DHS Certification No 1644 <br />