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I110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' jttp.Lwww mccampbell.com E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Repair <br /> Date Sampled 11/22/99 <br /> 4005 Nortb Wilson Way Date Received 11/23/99 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/23-11130199 <br /> Client P O Date Analyzed 11/23-11130199 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 26119 <br />' Client ID VW-4/11-22-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2800 trans-1,3-Dichloropropene ND<630 <br />' Benzene 15,000 Ethylene dibromide ND<630 <br /> Bromobenzene ND<630 Ethylbenzene 3800 <br /> Bromoch]oromethane ND<630 Hexachlorobutadiene ND<630 <br />' Bromodichloromethanc ND<630 lodomethane ND<630 <br /> Bromoform ND<630 ]sopropylbenzene ND<630 <br /> Bromomethane ND<630 p-Isopropyl toluene ND<630 <br /> n-Butyl benzene ND<630 Methyl butyl ketone` ND<630 <br />' sec-Butyl benzene N13<630 Methylene Chloride"' ND<640 <br /> tert-Butyl benzene ND<630 Methyl ethyl ketone ND<630 <br /> Carbon Disulfide ND<630 Methyl isobutyl ketone a ND<630 <br /> Carbon Tetrachionde ND<630 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<630 Naphthalene ND<630 <br /> Chloroethane ND<630 n-Propyl benzene ND-630 <br /> 2 Chloroethyl Vinyl Ether` ND<630 Styrene ND<630 <br /> Chloroform ND<630 1,1,1,2-Tetrachloroethane ND<630 <br /> Chloromethane ND<630 1,1,2,2-Tetrachloroethane ND<630 <br /> 2-Chiorotoluene ND<636 Tetrachloroethene ND<630 <br /> 4-Chlorotoluene ND<630 Toluene'° 18,000 <br /> Dibromochloromethane ND<630 1,2,3 Tnchlorobenzene ND<630 <br /> 1,2-Dibromo-3-chloropropane ND<630 1,2,4-Tnchlorobenzene ND<630 <br /> Dibromomethane ND<630 1,1,1-Tnchloroethane ND<630 <br /> 1,2-Dichlorobenzene ND<630 1,1,2-Trichloroethane ND<630 <br /> 1,3-Dichlorobenzene ND<630 Tnchloroeihene ND<630 <br />' 1,4-Dichlorobenzene ND<630 Trichlorofluoromethane ND<630 <br /> Dichlorodifluoromethane ND<630 1,2,3-Tnchl oropropane ND<630 <br /> l,]-Dichloroethane ND<630 1,2,4-Tnmethylbenzene 2900 <br /> 1,2-Dichloroethane ND<630 1,3,5-Tnmethylbenzene 780 <br />' 1,1-Dichloroethene ND<630 Vinyl Acetate`° ND<630 <br /> cis-1,2 Dichloroethene ND<630 Vinyl Chloride ND<630 <br /> trans-],2-Dichloroethene ND<630 Xylenes,total 'P18,000 <br />' 1,2-Dichloropropane ND<630 Comments <br /> 1,3-Dichloropropane ND<630 Surrogate RecoN cries(%) <br /> 2,2-Dichloropropane ND<630 Dibromofluoromethane 96 <br /> ],1-Dichioropropene ND<630 Toiuene-d8 102 <br /> cis-1,3-Dichlompropene ND<630 4-Bromofluorobenzene 89 <br />' water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ugi .apor samples 0 5 ug/L,solid and sludge samples 5 ug/kg wipes 0 2ug/..ipe <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlaroethoxy) ethene, (d) 2-hexanvne, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —S vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Cerhfication No 1644 Edward Hamilton, Lab Director <br />