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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925.798-1620 Fax 925-798-1622 <br />' httn//www mceampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Protect ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br />' Stockton, CA 95215 Client Contact Calvm Lee Date Extracted 11/16-11/21/01 <br /> Client P O Date Analyzed 11116-11/21/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 83761 <br />' Client ID CPT-2-145 <br /> Matrix W <br /> Compound Concentration* Reportng Limit Compound Concentration* Rc[wrung Lima <br />' W S W S <br /> Acetone ro ND<500 50 25 trans-l,3-Dichloropropene NIX100 10 50 <br /> Benzene 680 i 1 0 50 Ethylene dibromide ND<100 10 5 0 <br /> Bromobenzene NIK100 1 0 50 Ethylbenzene 1600 1 0 __5_0_1 <br /> 1 Bromochlaromethane ND<100 1 0 50 Hexachlorobutadiene ND<500 5 0 25 <br /> Bromodichloromethane ND<100 1 0 5 0 lodomethane ND<100 1 0 5 0 <br /> BiomOfOrm N13<100 1 0 5 0 Isopropylbenzene ND<100 10 5 0 <br /> Bromomethane ND<100 1 0 5 0 p-Isopropyl toluene ND<100 1 0 50 <br />' n-Butyl benzene ND<100 1 0 5 0 Methyl butyl ketone(d) ND<100 10 5 0 <br /> sec-Butyl benzene ND<100 1 0 50 Methylene Chloride"' ND<100 10 5 0 <br /> tert-Butyl benzene ND<100 1 0 5 0 Methyl ethyl ketone ND<200 2 0 10 <br /> Carbon Disulfide ND<100 1 0 50 Methyl isobutyl ketones ND<100 10 50 <br /> l <br /> Carbon Tetrachloride ND<100 1 0 5 0 Methyl tert-Butyl Ether(MTBE) - to 50 <br /> ie Chlorobenzene N13<100 1 0 5 0 Naphthalene 980 5 0 25 <br /> Chloroethane N13<I00 1 0 5 0 n-Propyl benzene 390 10 5 0 <br /> 2-Chloroethyl Vinyl Ether" ND<100 1 0 5 0 Styrene ND<100 1 0 50 <br /> Chloroform ND<100 1 0 5 0 1,1,1,2-Tetrachloroethane ND<100 10 5 0 <br /> Chloromethane ND<l00 1 0 5 0 1,1,2 2-Tetrachloroethane ND<100 1 0 5 0 <br /> 2-Chlorotoluene ND<100 10 5 0 Tetrachloroethene N13<I00 1 0 5 0 <br /> 4-Chlorotoluene ND<100 10 5 0 Toluene M 5300 10 50 <br />' Dibromochloromethane ND<100 1 0 50 1,2,3-Tnchlorobenzene ND<500 50 25 <br /> 1,2-Dibromo-3-chloropropane ND<200 2 0 10 1,2,4-Tnchlorobenzene ND<500 5 0 25 <br /> Dibromomethane ND<100 1 0 5 0 1,1,1-Tnchlomethane N13<100 1 0 50 <br /> 1,2-Dichlorobenzene ND<100 10 50 1,1,2-Trichloroethane ND<100 10 5 0 <br /> 1,3-Dichlorobenzene ND<100 1 0 50 Trichloroethene ND<100 1 0 50 <br /> 1,4-Dichlorobenzene ND<100 1 0 5 0 Tnchlorofluoromethane ND<100 10 50 <br /> Dichlorodifluoromethane ND<100 to 5 0 1,2,3-Tnchlonopropane ND<100 t 0 5 0 <br /> l,l-Dichloroethane ND<100 to 50 1,2,4-Tnmethylbenzene 2500 10 1 5 0 <br />' 1,2-Dichloroethane NI3<100 1 0 5 0 1,3,5-Tnmethylbenzene 730 1 0 5 0 <br /> 1,1-Dichlomcthene ND<100 1 0 5 0 Vinyl Acetate m ND<500 5 0 25 <br /> cis-1,2-Dichloroethene ND<100 1 0 5 0 Vinyl Chloride " ND<100 10 5 0 <br /> trans-1,2-Dichloroethene ND<100 1 0 5 0 Xylenes,total 7900 1 0 5 0 <br />' 1,2-Dichloropropane ND<100 10 50 Comments <br /> 1,3-Dichloropropane ND<100 10 5 0 Surrogate Recoveries(%) <br /> 2 2-Dichloropropane ND<100 10 50 Dibromofluoromethane Ll <br />' 1,1-Dtchloropropene ND<100 1 0 5 0 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<100 10 50 4-Brorrrotluorobenzene 101 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />