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1 <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell com E-mail main@mccampbell com <br /> • <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 11/16-11/21101 <br /> Client P O Date Analyzed 11/16-11121/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 83762 <br /> Client ID CPT-2-155 <br /> Matrix W <br /> Repcitng Limit RcWmng Lunt <br /> Compound Concentration* W S Compound Concentration* W S <br />' Acetone 1b) ND<250 50 25 trans-l,3-Dichloropropene ND<50 l 0 5 0 <br /> Benzene 360 ] 0 50 Ethylene dibromide ND<50 1 0 50 <br /> Bromobenzene ND<50 to 5 0 Ethylbenzene 860 10 50 <br /> Bromochloromethane ND<50 to 5 0 Hexachlorobutadiene ND<250 _5__O 25 <br /> Bromodichloromethane ND<50 10 50 Iodomethane ND<50 1 0 50 <br /> Bromoform ND<50 10 5 0 ]sopropylbenzene 61 / 1 0 5 0 <br /> Bromomethane ND<50 10 5 0 p-Isopropyl toluene ND<50 1 0 50 <br /> n-Butyl benzene ND<50 10 5 0 Methyl butyl ketone ND<50 1 0 50 <br /> sec-Butyi benzene ND<50 10 50 Methylene Chloride° ND<50 10 5 0 <br /> tert-Butyl benzene ND<50 10 5 0 Methyl ethyl ketone ND<100 2 0 10 <br /> Carbon Disulfide ND<50 10 50 Methyl isobutyl ketone a ND<50 10 50 <br /> Carbon Tetmchlonde ND<50 to 50 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlombenzene ND<50 10 5 0 Naphthalene 490 50 25 <br /> Chloroethane ND<50 10 50 n-Propyl benzene 260 1 0 50 <br />' 2-Chloroethyl Vinyl Ether"' ND<50 10 50 Styrene M ND<50 1 0 50 <br /> Chloroform ND<50 10 50 1,1,1,2-Tetrachloroethane N13<50 I O 5 0 <br /> Chloromethane ND<50 10 50 1,1,2,2-Tetrachloroethane ND<50 10 5 0 <br /> 2-Chlorotaluene ND<50 10 5 0 Tetrachloroethene ND<50 1 0 5 0 <br /> 4-Chlorotoluene ND<50 10 50 Toluene 3200 1 0 50 <br /> Dibromochlvromethane ND<50 --2-51 <br /> 1 0 50 1,2,3-Trichlorobenzene ND<250 5 0 <br /> 1,2-Dibromo-3-chloropropane ND<100 2 0 10 1,2,4-Trichlorobenzene ND<250 5 0 25 <br /> Dibromomethane ND<50 1 0 5 0 1,1,1-Trichloroethane NLX50 1 0 50 <br />' 1,2-Dichlorobenzene ND<50 to 5 0 1,1,2-Tnchloroethane ND<50 1 0 50 <br /> 1,3-Dichlorobenzene ND<50 10 5 0 Trichloroethene ND<50 1 0 5 0 <br /> 1,4-Dichlorobenzene ND<50 10 50 Tnchlorofluoromethane ND<50 1 0 5 0 <br /> Dichlorodifluoromethane ND<50 1 0 50 1,2,3-Tnchloropropane N1X50 1 0 50 <br />' 1,1-Dichloroethane ND<50 10 50 1,2,4-Tnmethylbenzene 1500e 10 50 <br /> 1,2-Dichloroethane ND<50 1 0 50 1,3,54nmethylbenzene 470 1 0 5 0 <br /> IJ-Dichloroethene ND<50 10 50 Vinyl Acetate"I ND<250 50 25 <br /> cis-1,2-Dichloroethene ND<50 10 50 Vinyl Chloride " ND<50 1 0 50 <br />' trans-1,2-Dichloroethene ND<50 10 50 Xylenes,total 4300 10 50 <br /> 1,2-Dichloropropane ND<50 to 50 Comments <br /> 1,3-DDichloropropane ND<50 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<50 10 50 Dibromofluoromethane 127 <br /> 1,1-Dichloropropene ND<50 1 0 50 Toluene-d8 101 <br /> cis-1,3-Dtchloropropene ND<50 1 0 50 4-Bromofluorobenzene 100 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanvne, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than –5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644Edward Hamilton,Lab Director <br />