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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' h //www mccam bell corn E-mail main@mccarnpbell corn <br /> • <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 11/16-11/21/01 <br /> CIient P O Date Analyzed 11/16-11/21/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 83763 <br /> Client ID CPT-3-58 <br /> Matrix W <br /> Repat�ng Urnit Pep°rtrtng Limit <br /> Compound Concentration* W S Compound Concentration* <br />' W S <br /> Acetone(b) ND<500 50 25 trans-1,3-Dichloropropene ND<100 1 0 50 <br /> Benzene 54001 1 0 50 Ethylene dibromide ND<100 1 0 50 <br /> Bromobenzene ND<100 10 50 Ethylbenzene 380 1 0 50 <br />' Bromochloromethane ND<100 1 0 50 Hexachlorobutadiene ND<500 50 25 <br /> Bromodichloromethane ND<100 10 50 lodomethane ND<100 1 0 50 <br /> Bromoform ND<100 10 50 Isopropylbenzene 140 10 50 <br /> Bromomethane ND<100 10 50 p-Isopropyl toluene ND<100 1 0 50 <br />' n-Butyl benzene ND<100 10 50 Methyl butyl ketone ND<100 to 50 <br /> sec-Butyl benzene ND<100 1 0 50 Methylene Chlonde` ND<100 1 0 —TO—] <br /> tert-Butyl benzene ND<100 1 0 50 Methyl ethyl ketone ND<200 20 10 <br /> . Carbon Disulfide ND<100 10 50 Methyl isobutyl ketones N13<100 1 0 50 <br />' Carbon Tetrachloride ND<100 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 so <br /> Chlorobenzene ND<100 10 50 Naphthalene ND<500 50 25 <br /> Chloroethane ND<100 10 5 0 n-Propyl benzene 300- 1 0 50 <br /> 2-Chloroethyl Vinyl Ether` ND<100 10 50 Styrene ND<100 1 0 50 <br />' Chloroform ND<100 1 0 50 1,1,1,2-Tetrachloroethane ND<100 1 0 50 <br /> Chloromethane ND<100 1 0 50 1,1,2,2-Tetrachloroethane ND<100 1 0 50 <br /> 2-Chlorotoluene ND<100 10 50 Tetrachloroethene ND<100 1 0 50 <br />' 4-Chlorotoluene ND<100 1 0 50 Toluene ND<100 1 0 50 <br /> Dibromochloromethane ND<100 10 50 12,3-Trichloroberizene ND<500 50 25 <br /> 1,2-Dibromo-3-chloropropane ND<200 20 10 1,2,4-Tnchlorobenzene ND<500 50 25 <br /> Dibromomethane ND<100 1 0 50 1,1,1-Tnchloraethane ND<100 1 0 50 <br />' 1,2-Dichlorobenzene ND<100 1 0 50 1,1,2-Tnehloroethane ND<100 1 0 50 <br /> 1,3-Dichlorobenzene ND<100 1 0 50 Trichloroethene ND<10ti 1 0 50 <br /> 1,4-Dichlorobenzene ND<100 10 50 Trichlorofluoromethane ND<100 1 0 50 <br /> Dichlorodifluoromethane N13<100 10 50 1,2,3-Trichloropropane ND<100 10 50 <br />' 1,1-Dichloroethane ND<100 1 0 50 1,2,4-Tnmethylbenzene ND<100 1 0 50 <br /> 1,2-Dichloroethane 190-1 10 50 1,3,5-Tnmethylbenzene ND<100 1 0 50 <br /> 1,1-Dichloroethene ND<100 10 50 Vinyl Acetate '° ND<500 50 25 <br /> cis-1,2-Dichlormthene ND<100 10 50 Vinyl Chloride " ND<100 1 0 50 <br />' trans-1,2-Dichloroethene ND<100 10 1 50 Xylenes,total ND<100 10 50 <br /> 1,2-Dichloropropane ND<100 10 50 Comments i <br /> 1,3-Dichloropropane ND<100 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<100 10 50 Dibromofluoromethane 120 <br />' 1,1-Dichloropropene ND<100 10 50 Toluene-d8 101 <br /> cis-1,3-Dichloropropene NEX100 1 0 50 4-Bramofluorobenzene 102 <br /> water and vapor samples are reported in-g/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than-5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />