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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http l/www mccampbell com E-mail mam@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 11/16-11/21101 <br /> Client P O Date Analyzed 11/16-11/21/01 <br />' Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 83765 <br />' Client ID CPT-3-I 17 <br /> Matrix W <br /> * Rrpartmg Lsmrt Reporting Limit <br /> Compound Concentration W S Compound Concentration* <br />' W S <br /> Acetone ca' ND 50 25 trans-1,3-01chloropropene ND 1 0 50 <br /> Benzene 32 1 0 5 0 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 50 <br />' Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 5 0 <br />' n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 —30 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride(.) ND 10 5 0 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone` ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyi ketone ND 1 0 5 0 <br />' Carbon Tetrachlonde ND 10 50 Methyl tent-Butyl Ether(MTBE) — 1 0 50 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 1 25 <br /> ChloroethaneND 10 5 0 n-Propyl benzene ND 10 5 0 <br />' 2-Chloroethyl Vinyl Ether" ND 1 0 50 Styrene ND 10 50 Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND to 5 0 Tetrachloroethene ND l 0 50 <br /> 4-Chlorotoluene ND I 0 5 0 Toluene ND 1 0 5 0 <br />' Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 5 0 t,1,1-Tnchloroethane ND 1 0 50 <br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 1 0 50 <br />' 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Tnchlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 10 50 <br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Trimethylbenzene 21 – 1 0 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzenc ND 1 0 50 <br /> l,I-Dichloroethene ND 10 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichioroethene ND 10 50 Vinyl ChlondeT"T ND 10 5 0 <br />' trans-l,2-Dichloroethene ND 16 50 Xylenes,total 21 - 1 0 5 0 <br /> 1,2-Dichlorcpropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 117 <br />' l,l-Dichloropropene ND 10 5 0 Toluene-d8 99 <br /> cis-1,3-Dichlorapropene ND 10 1 50 4-Bromofluorobenzene L 108 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vipe and all TCLP/SPL.P extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 �EdwardHamilton,Lab Director <br />