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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MICA DBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamt)bell co m E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Protect ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br /> IStockton, CA 95215 Client Contact Calvm Lee Date Extracted 11/16-11121101 <br /> Client P O Date Analyzed 11/16-11/21101 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 83766 <br />' Client ID CPT-3-156 <br /> Matrix W <br /> Reporting Limit Reporting Limit <br /> Compound Concentration* W S Compound Concentration* W S <br />' Acetone(b) ND 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene 50 1 0 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene STD 1 0 50 Ethylbenzene 16 1 0 50 <br />' Bromochloromethane ND 1 0 50 Hexachlorobutadlene ND so 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 50 isopropylbenzene 28 10 50 <br /> Bromomethane ND 1 0 50 p4sopropyl toluene ND 1 0 50 <br />' n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene 1 1 / 1 0 50 Methylene Chloride"' ND 10 50 <br /> tart-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketones ND 10 50 <br /> Carbon Tetrachlonde ND 1 0 50 Methyl tent-Butyl Ether(MTBE) 10 so <br /> Chlorobenzene ND 1 0 50 Naphthalene 5 7 - 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene i 92 - 1 0 50 <br /> 2-Chloroethyl Vinyl Ether7T ND 1 0 50 Styrene ND 10 50 <br />' Chloroform ND to 50 1,1,1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chtorotoluene ND 1 0 50 Tetrachloroethane ND 10 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene 29 ` 10 50 <br />' Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 1 0 5 0 <br />' 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 1 0 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 50 Tnchloraethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorotluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 1 0 5 0 <br />' 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene 39 1 0 5 0 <br /> 1,2-Dichloroethane 3 5 ' 1 0 50 1,3,5-Tnmethylbenzene 13 1 0 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND 1 0 5 0 <br /> trans-1,2-Dichloroethene ND to 50 Xylenes,total 68 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments t <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane hfl17 <br /> 1 1-Dichloropropene ND 10 50 Toluene-dg 99 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bromofluorobenzene 05 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --�5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (in) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />