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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell coin E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 11/13/01 <br /> 837 Shaw Road Date Received 11/16/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11/16-11/21/01 <br /> Client P O Date Analyzed 11/16-11/21/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 83767 <br /> t Client ID CPT-3-178 <br /> Matrix W <br /> Rcparting Limit Reporting Limit <br /> Compound Concentration* S Compound Concentration* W S <br />' Acetone 7 ND 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene 20 -1 10 50 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 5 0 <br />' Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 1 0 5 0 <br /> Bromoforrn ND 1 0 5 0 Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride"' ND 10 5 0 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone MND 2 0 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketones ND 1 0 50 <br /> lieCarbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) — 10 50 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 50 25 <br /> Chloroethane ND 10 5 0 n-Propyl benzene 1 3 `d50 <br /> 50 <br /> 2-Chloroethyl Vinyl Eth ` ND 10 5 0 Styrene ND 50 <br />' Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 5 0 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 5 0 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 50 <br /> 4-Chlorotoluene ND 10 50 Toluene ND 5 0 <br />' abromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Trichlorobenzene ND 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 1 0 50 <br />' 12-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND to 50 <br /> 1,3-Dtchlorobenzene ND 1 0 5 0 Tnchloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Tnchlomfluoromethane ND to 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tncbloropmpane ND 10 50 <br />' 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene 54 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene 19 10 50 <br /> l,l-Dichloroethene ND 10 5 0 Vinyl Acetate m ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride ND 1 0 50 <br />' trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total 50 10 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 116 <br />' I,1-Dichloropropene ND 10 50 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 10 50 1, 4-Bromofluorobenzene 107 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (1) liquid sample that contains greater than--5 vol 0/6 <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, O methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />