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Surrogate Spike Recovery <br /> The surrogate %recoveries were within the control limits as indicated in the report <br /> provided by Calscience. <br /> Matrix Spike, Matrix Spike Duplicate,the Relative Percent Differences, <br /> The MS and MSD were analyzed with the sample and the percent recoveries and the <br /> RPDs were within the control limits. <br /> Laboratory Control Sample <br /> LCS samples analyzed with the sample batch and were within control limits as stated by <br /> Calscience. <br /> Diesel in Soil - Modified EPA Method— M8015D <br /> Holding Times <br /> The holding time for the analysis of soil is 14 days and . All samples were analyzed <br /> within this time period meeting the above requirements. <br /> Method Blanks <br /> A method blank was analyzed with the same batch as the sample. No contamination was <br /> found. <br /> Sensitivity <br /> The sample was diluted by a factor of 5. The RL was adjusted for this dilution. <br /> Surrogate Spike Recovery <br /> The surrogate %recoveries were within the control limits indicating no compound of <br /> interest was lost during the analytical procedure. <br /> Matrix Spike,Matrix Spike Duplicate and the Laboratory Control <br /> The MSs, MSDs the RPDs and the LCSs %recoveries reported were within the control <br /> limits. <br /> Motor Oil in Soil Modified EPA Method—M 8015B <br /> Holding Times <br /> The holding time for the analysis is twenty eight days for soil. The samples were <br /> analyzed within this time period meeting this requirement. <br /> Method Blanks <br /> The method blank was analyzed with the sample A-3-2-1 and no contamination was <br /> detected. <br /> Sensitivity <br /> A dilution factor of 3 was necessary and therefore the RL was adjusted to this factor. <br /> 12 <br />