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real-time leak detection activities, using helium as the tracer compound, be conducted as part of <br /> the Phase 2 sampling activities. <br /> For the RI portion of this project (Phase 1), the compound used as the tracer was isobutane in the <br /> form of Barbasol® shaving cream. During the SSI (Phase 2), helium was used as the real time <br /> leak detection compound. Details of the procedures for leak detection determination used at the <br /> Site during the RI and SSI are provided in subsequent sections: <br /> Phase I Leak Detection Compound—Isobutane <br /> To determine if there were leaks in the soil gas sampling system, Barbasol® shaving cream <br /> containing isobutane was applied to the top of each boring prior to sampling as a leak-check <br /> compound (DTSC, 2003). At the point where the soil gas sample tubing daylights at the surface <br /> in each boring location, the shaving cream was sprayed in the well box until the soil gas tubing <br /> and the ground, where it daylighted, was completely covered. Additionally, the shaving cream <br /> was placed at each connection point in the sampling system. The shaving cream was sprayed <br /> into a clean, dry rag that was secured around the connection points in the system such that any <br /> leaks in the system would be detected. The samples were then analyzed for isobutane to <br /> determine if there is a leak in the system (i.e., if isobutane is detected above the Advisory <br /> guidance of 10 micrograms per liter(ug/L), the system has a leak). <br /> Phase 2 Real-Time Leak Detection Compound—Helium <br /> Real-time leak testing procedures using helium as the tracer compound were accomplished as <br /> follows: <br /> 1. The tracer gas compound was introduced around the sample probe and canister by filling <br /> a shroud positioned over the sample location. <br /> 2. The shroud was suitably sealed to the ground surface. <br /> 3. The tracer gas was introduced into the shroud. Helium was injected into the shroud at a <br /> maximum of 5 pounds per square inch. The shroud had a valve fitting at the top of the <br /> chamber to introduce the tracer gas into the shroud and a valve fitting at the bottom to let <br /> the ambient air out while introducing tracer gas. The helium concentration within the <br /> shroud was monitored with a field helium detector and maintained at>30%. <br /> 4. The shroud had a gas-tight fitting or sealable penetration to allow the soil vapor sample <br /> probe tubing to pass through and exit the chamber. <br /> 5. The sample probe tubing exiting the shroud was attached to a pump that was pre- <br /> calibrated to extract soil vapor at a rate of 200 ml/min. <br /> 6. Prior to collecting the sample in the canister, leak detections samples were collected in a <br /> 1-liter Tedlar bag. The Tedlar bag sample was analyzed with the handheld helium <br /> detector for the tracer gas and the detected concentrations were recorded on a field <br /> summary sheet. If the concentration of the tracer was >10% of the concentration <br /> measured from the shroud, the probe was re-sealed. The tracer test was performed again, <br /> and sample collection proceeded when the tracer concentration was <10% of the <br /> concentration in the shroud. <br /> 7. Following collection of the sample in the Summa canister, an additional soil gas sample <br /> was collected in a Tedlar bag and monitored for helium. If both the pre- and post- <br /> sampling Tedlar® bag samples contain helium at <10% of the shroud concentration, then <br /> the sample passed the leak test. If not, additional corrective measures were undertaken in <br /> PARSONS 23 FINAL RI REPORT-FORMER TRACY MGP <br /> APRIL 2010 <br />