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KD (70Sequoia. 1455Mcl7owc13Blvd North Ste <br /> Petaluma CA 949544 <br /> Analytical FAX <br /> 7)792-1865 <br /> (707)792-0342 <br /> www sequoialabs com <br /> ettler-Ryan Inc Project TOSCO/PHILLIPS <br /> 364 North Me Dowell Blvd,Suite B2 Project Number 6981 /STOCKTON,CA Reported <br /> Petaluma CA,94954-1116 Project Manager Clyde Galantine 11/30/01 17 13 <br /> Total Petroleum Hydrocarbons as Gasoline and BTEX by EPA 8015M/8020M -Quality Control <br /> Sequoia Analytical- Petaluma <br /> Reporting Spike Source %REC RPD <br /> [Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1110514-EPA 5030,soils <br /> Blank(1110514-BLKI) Prepared&Analyzed 11/20/01 <br /> Gasoline(C6-C12) ND 1 0 mg/kg <br /> Benzene ND 00050 " <br /> Toluene ND 00050 " <br /> Ethylbenzene ND 00050 " <br /> Xylenes(total) ND 00050 " <br /> Methyl tert-butyl ether ND 0 050 " <br /> Surrogate a a a-Trifluororoluene 0 597 0 600 100 65-135 <br /> Surrogate 4-Bromofluorobenzene 0 627 0 600 104 65-135 <br /> Blank(1110514-BLK2) Prepared&Analyzed 11/21/01 <br /> Gasoline(C6-C12) ND 1 0 mg/kg <br /> eene ND 00050 <br /> ruene ND 00050 " <br /> Ethylbenzene ND 00050 " <br /> Xylenes(total) ND 00050 " <br /> Methyl tert-butyl ether ND 0 050 " <br /> Surrogate a a a-Trifluorotoluene 0 590 0 600 98 65-135 <br /> Surrogate 4 Bromofluorobenzene 0 650 0 600 108 65-135 <br /> LCS(1110514-BS1) Prepared&Analyzed 11/20/01 <br /> Gasoline(C6-C 12) 5 57 10 mg/kg 5 50 101 65-135 <br /> Benzene 00827 00050 00660 125 65-135 <br /> Toluene 0 393 00050 0 397 99 65-135 <br /> Ethylbenzene 00886 00050 00920 96 65 135 <br /> Xylenes(total) 0 485 00050 0 461 105 65 135 <br /> Methyl tert-butyl ether 0 135 0 050 0 105 129 65-135 <br /> Surrogate a a a-Trifluorotoluene 0 591 0 600 98 65-135 <br /> Surrogate 4 Bromofluorobenzene 0 652 0 600 109 65-135 <br /> O <br /> uola Analytical-Petaluma The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 4 of 7 <br />