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1455McDowcll Blvd North Ste D <br /> Sequoia Pctaluma CA 94954 <br /> (707)792-1865 <br /> TOW Analytical FAX(707)792-0342 <br /> www sequoialabs corn <br /> t <br /> ttler-Ryan Inc Project TOSCO/PHILLIPS <br /> 64 North Me Dowell Blvd,Suite B2 Project Number 69811 STOCKTON,CA Reported <br /> taluma CA,94954-1116 Project Manager Clyde Galantine 11/30/01 17 13 <br /> Total Petroleum Hydrocarbons as Gasoline and BTEX by EPA 8015M18020M - Quality Control <br /> Sequoia Analytical- Petaluma <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1110514-EPA 5030, soils <br /> LCS(1110514-BS2) Prepared&Analyzed 11/21/01 <br /> Gasoline(C6-C12) 564 1 0 mg/kg 5 50 103 65-135 <br /> Benzene 00840 00050 00660 127 65-135 <br /> Toluene 0 403 00050 0 397 102 65-135 <br /> Ethylbenzene 00907 00050 00920 99 65-135 <br /> Xylenes(total) 0 497 00050 0 461 108 65-135 <br /> Methyl cert-butyl ether 0 140 0 050 0 105 133 65-135 <br /> Surrogate a a a-Trifluorotoluene 0 597 0 600 100 65-135 <br /> Surrogate 4-Bromofluorobenzene 0 658 0 600 110 65-135 <br /> Matrix Spike(1110514-MSI) Source P111441-01 Prepared&Analyzed 11/20/01 <br /> Gasoline(C6-C12) 566 10 mg/kg 5 50 ND 102 65-135 <br /> zene 00710 00050 00660 ND 111 65-135 <br /> uene 0 430 00050 0 397 ND 108 65-135 <br /> Ethylbenzene 00965 00050 00920 ND 105 65-135 <br /> Xylenes(total) 0 523 00050 0 461 ND 113 65-135 <br /> Methyl tert-butyl ether 0 120 0 050 0 105 ND 114 65-135 <br /> Surrogate a a a-Trac luorotoluene 0 611 0 600 104 65-135 <br /> Surrogate 4-Bromofluorobenzene 0 617 0 600 103 65-135 <br /> Matrix Spike Dup(1110514-MSD1) Source P111441-01 Prepared&Analyzed 11/20/01 <br /> Gasoline(C6-C 12) 531 10 mg/kg 550 ND 95 65-135 6 20 <br /> Benzene 00762 00050 00660 ND 115 65-135 4 20 <br /> Toluene 0 431 00050 0 397 ND 108 65-135 0 2 20 <br /> Ethylbenzene 00982 00050 0 0920 ND 107 65-135 2 20 <br /> Xylenes(total) 0 529 00050 0 461 ND 115 65-135 1 20 <br /> Methyl tert-butyl ether 0 122 0 050 0 105 ND 116 65-135 2 20 <br /> Surrogate a a a-Trifluorotoluene 0 623 0 600 104 65-135 <br /> Surrogate 4-Bromofluorobenzene 0 575 0 600 96 65-135 <br /> u0i a Analytical-Petaluma The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 5 of 7 <br />