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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamnbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project 1D Grantline Gas And Date Sampled 09/20/99 <br /> 4005 North Wilson Way Food Date Received 09/23/99 <br />' Stockton, CA 95205 Client Contact Bill Little Date Extracted 09/23-09129199 <br /> Client P O Date Analyzed 09123-09/29/99 <br />' Oxygenated Volatile Organics By GUMS <br /> EPA method 8264 modified <br />' Lab ID 19829 19830 19831 19832 <br /> MW1/9-20- MW2/9-20- MW3/9-20- MW4/9-20- Reporting Limit <br /> Client ID 99 99 99 99 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPE) ND<5 ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<5 ND ND ND 50 10 <br />' Methyl-tert Butyl Ether(MTBE) 170 ND 2 1 81 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<5 ND ND ND 50 1 0 <br />' tert-Butanol ND<25 ND ND ND 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 101 97 99 97 <br /> Comments h <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment 0)sample diluted due to <br /> high organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />