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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MICA OBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' hqp//www mcca=bell com E-mail mam@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Grantlme Gas And Date Sampled 09/20/99 <br /> 4005 North Wilson Way Food Date Received 09/23/99 <br />' Stockton, CA 95205 CIient Contact Bill Little Date Extracted 09/23-09/29/99 <br /> Client P O Date Analyzed 09/23-09/29/99 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> LabID 19833 19834 19835 19836 <br />' Client ID MW5/9-20- MW6/9-20- MW7/9-20- MW8/9-20- Reporting Limit <br /> 99 99 99 99 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(D1PE) ND ND ND ND 50 10 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND so 10 <br /> Methyl-tert Butyl Ether(MTBE) 87 ND 77 ND so 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> Itert-Butanol ND ND ND ND 25 so <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 95 101 101 93 <br /> Comments h <br />' •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />