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110 Second Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br />' Client Project ID #0111, Grantline Gas& Date Sampled 06/18/98 <br /> Advanced GeolJnvtronmental J <br /> 4005 North Wilson Way Food Date Received 06/20/98 <br />' <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/25/98 <br />' <br /> Client P O Date Analyzed 06/25/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 90883 <br /> Client ID MW3/6-18-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone lb' NIX5 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br />' Bromochloromethane ND I sopropyl benzene ND <br /> Bromodichloromethane ND p4sopropyl toluene ND <br /> Bromoform ND Methyl butyl ketoneND <br /> Bromomethane ND Methylene Chloride" ND <br /> n-Butyl benzene ND Methyl ethyl ketoneND <br /> sec-Butyl benzene ND Methyl isobutyl ketone's ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) - <br /> Carbon Disulfide ND Naphthalene ND<15 <br />' Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene' ' ND <br /> Chloroethane ND 11 12-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ethe ND 1,1 2,2-Tetrachloroethane ND <br />' Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene` ND <br /> 2-Chlorotoluene ND 1 2 3-Trichlorobenzene ND <br />' 4-Chlorotoluene ND 1,2 4-Trichlorobenzene ND <br /> Dibromochloromethane ND 11 I-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,12-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br />' 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1 2 3-Tnchloropropane ND <br /> 1,4-Dichlorobenzene ND 1 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3 5-Trimethylbenzene ND <br />' I I-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"' ND <br /> 1,1-Dichloroethene ND Xylenes total '°' ND <br /> cis-1,2-Dichloroethene ND <br />' trans-1,2-Dichloroethene ND <br /> 1 2-Dichloropropane ND <br /> 1 3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br />' 1,1-Diehl oropropene ND Surrogate Reco%eries <br /> cls-1,3-Dichloropropene ND Dibromolluoromethane 115 <br /> trans-1,3-Dichloropropene ND Toluene-d8 106 <br /> Ethylene dibromrde ND 4-Bromotluorobenzene 99 <br />' water and vapor samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 o ug/L vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone, (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br />' pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol °/a <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte,(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 -Edward Hamilton, Lab Director <br />