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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> • http//www mccap2Rt t com E-mail main@mccampbell com <br />' Client Project ID ##0111,Grantline Gas& Date Sampled 06/18/98 <br /> Advanced GeoEnvironmental ! <br /> 4005 North Wilson Way Food Date Received 06/20/98 <br />' <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/25/98 <br />' Client P O Date Analyzed 06/25/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90884 <br /> Client ID MW4/6-18-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone ND<5 Ethylbenzene ND <br /> Benzene 18 Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chloride" ND <br />' n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'x ND <br /> Cert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) - <br />' Carbon Disulfide 59 Naphthalene N13<15 <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene' ND <br /> Chloroethane ND 1,1,1 2-Tetrachloroethane ND <br />' 2-Chloroethyl Vinyl Ether" ND 1 1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene' ND <br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND <br />' 4-Chlorotoluene ND 12,4-Tnchlorobenzene ND <br /> Dibromochloromethane ND 1,1 1-Ti ichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,12-Trichloroethane ND <br /> Dibromomethane ND Tnchloroethene ND <br />' 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1 2 3 Tricliloropropane ND <br /> 1,4-Dichlorobenzene ND l 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Diehl oroethane ND Vinyl Acetate"" ND <br />' 1,2-Dichloroethane ND Vinyl Chloride ND <br /> 1,1-Dichloroethene ND Xylenes,total '°' ND <br /> cis-1,2-Dichloroethene ND <br />' trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments h <br />' 1,1-Dichloropropene ND Surrogate Recoveries('%) <br /> cis-1,3-Dichloropropene ND Dibromotluoromethane 117 <br /> trans-1,3-Dichloropropene ND Toluene-d8 107 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 103 <br />' *water and vapor samples are reported In ug/L,soil and sludge samples m ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts to ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone, (e)dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br />' pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than ,5 vol % <br /> sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte,(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Cernficahon No 1644 // Edward Hamilton,Lab Director <br />