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�i 4o g <br /> 110 2nd Ave South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell corn E-mail main@mccampbell corn <br /> J <br /> GI ound Zero Analysis, Inc <br /> Client Project ID #95-013, Knowles- Date Sampled 07/14/98 <br /> 1714 Main Street Hammer Date Received 07/23/98 <br /> Escalon, CA 95320 Client Contact Jeanne Bucicthal Date Extracted 07/23/98 <br /> Client P O Date Analyzed 07/25-07/26/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92657 <br /> Client ID S-DBI-66 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<20 Ethylbenzene 120 <br /> Benzene 170 Hexachlorobutadiene ND<15 <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND I Isopropylbenzene 95 <br /> Biomodichloromethane ND p-Isopropyl toluene ND <br /> Bromotorrrt ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene 32 Methyl ethyl ketone' ' ND <br /> Su.-Butyl benzene 68 Methyl isobutvl ketone`s ND <br /> teri-Butyl benzene ND Methyl teat-Butyl Ether(MTBE) - <br /> Carbon Disultide ND Naphthalene ND<30 <br /> Carbon Tetrachloride ND ii-Propyl bLI1ZLne 47 <br /> Chlorobcnzcne ND Styruu' ND <br /> Chloroethane ND I 112-TLtIaLh1010ethane ND <br /> 2-Cbloroethyl Vinyl Ether"' ND 1 1 2 2 TLtiachloroethane ND <br /> Chlorotorm ND Tettachloinethene ND <br /> C hloromethane ND I01ULTIe" 530 <br /> 2-Chloiotoluene ND 1 2 3-Tnchlorobenzene ND<30 <br /> 4 Chlorotoluene ND 1 2 4-Ti1Lh10roben7ene ND<15 <br /> Dibromochloromethane ND I I 1-lnchloioethane ND <br /> 12-Dibromo-3-chloropropane ND l i 2-Trichloroethane ND <br /> Dibiomomethane ND TrlchlorOtlhcnc ND <br /> 1 2-Dich1orobenzene ND TrichloiOlIL101omethane ND <br /> 13-Dichlorobenzene ND 1 2 3 Tauhloropiopane ND <br /> 14-Dichlorobenzene ND 1 2 4-Fiimethylbenzene 240 <br /> Dichlorod111uorometh ane ND 1 3 5 Tt1mCIII�IbLnzene 82 <br /> 1 i-Dichloruethant. ND Vmyl ALL1,11L 20 <br /> 1 2 DichloioethanL ND VIIIVI(hlotidL"" ND <br /> l i-Dichlorcethene ND Xyk,ncs total "" 590 <br /> cis-] 2 Drchloroethene ND <br /> trans-1 2-Drchloroethene ND <br /> I 2-Dichloropropane ND <br /> I 3-Dichloropropane ND <br /> 2 2-Dichloropropane ND Comments <br /> I I-Dichloropropene ND Surrogate Recoveries(°/) <br /> cis-1 3 Dichloropropene ND Dibiomotluoiomethane 106 <br /> trans-13-Dichloropropene ND Toluene-d8 97 <br /> Ethvlenedibromide ND i 4-131 omotluoaobenzene 101 <br /> water and vapor samples are reported in ug/L. soil and sludge samples in ug/kg �%ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapoi samples 0 5 ug/L solid and sludge samples 5 0 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit N/A mean~analyti,1101 apphLablc to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-ehloroethoxy) etl1Lnc (d) 2-hexanone (e) dichloromethane (t) 2 butanone (g) 4-methyl-2- <br /> pentanone of isopropyl acetone (h) lighter than water immiscibly sheen is present (i) Iryuad sample that Wiltains greater than --5 vol % <br /> sediment (1)sample diluted due to high organic content (k)peaks plea nt m this carbon r ange do not match (lie pattern of our standard for <br /> this analvtc (1)methylbenzene (m)acetic acid ethenyl ester (n)ch10i0L1hutc (o)drmethylbenzcnes <br /> DHS Certification No 1644 /i Ed"aid Hamilton, Lab Director <br />