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t li v <br /> 1 10 2nd Ave South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 http//www mccampbell com E-mail main@mccampbell cam <br /> JClient Pro ect ID #95-013, Knowles- Date Sampled 07/14/98 <br /> Ground Zero Analysts, Inc <br /> 1714 Main Street Hammer Date Received 07/23/98 <br /> Escalon, CA 95320 Client Contact Jeanne Buckthal Date Extracted 07/23/98 <br /> Client P O Date Analyzed 07/25-07/26/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92658 <br /> Client ID S-DBI-98 5 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ' ND<20 Ethylbenzene 10 <br /> Benzene 7 9 Hexachlorobutadiene ND<15 <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopiopyl toiuene ND <br /> Bromotorm ND Methyl butyl ketone... ND <br /> Biomomethane ND Methylene Chionde" ND <br /> ii-Butyl benzene ND Methyl ethyl ketone" ND <br /> Su.-Butyl benzene ND Methyl isobutyl ketone`s ND <br /> tert-Butyl benzene ND Methyl tort-ButvI Ether(MTBE) <br /> Cai bon Disulfide ND NaplithalenL ND<30 <br /> Cai bon Teti achloiide ND n Piopvl benzene ND <br /> Cil oro henzene ND Stviene' ND <br /> Chloroethane ND l 1 1 2-Ten acli loi oethane ND <br /> 2-Chloioethyl Vinyl Ether"' ND 1 1 2 2-TLnaLhl0Ioethine ND <br /> Chlorotorm ND Tetrachloioethene ND <br /> C hloromethane ND Toluene'' 32 <br /> 2-Chlorotoluene ND l 2 3-Ti Iehlorobenzene ND<30 <br /> 4-Chlorotoluene ND 124-Trichlorobenzene ND<15 <br /> Dibromochloromethane ND l I 1-Tiichlowethane ND <br /> l2-Dibrorno-3-chloropropane ND l l2-Trichloroethane ND <br /> Dihromomethane ND TrichloroethLne ND <br /> l 2 Dichlorobenzene ND TrllhloroflnnSomethane ND <br /> 13-Dichlorobenzene ND 1 2 3-Ti ichloropiopane ND <br /> l 4 Du.hlorobenzene ND 1 2 4-Ti imethvlbenzene 21 <br /> DichloinditlUmiomethane ND l 3 D-TIlmLthVlberzene 96 <br /> I l-Du.hloroethane ND Vinyl Acetate""' ND <br /> I 2-Dichloroethane ND Vmyi Chlnrula,"" ND <br /> I I-Dichloroethene ND Xylenes total `°' 48 <br /> CLS-1 2-Dichloroethene ND <br /> h ans-1 2-Dichiamethene ND <br /> l 2-Dichloropropane ND <br /> t 3-Dichloropropane ND <br /> 2 2-Dichloropropane ND CommEnts <br /> I 1-Drchloropropene ND Surrogate Recoveries('%.) <br /> Lis-13-Diehloropropene ND DlbromotlilolDnlethane 102 <br /> tian5-1 3-Dichloropropene ND Toluene-db 97 <br /> Ethylene dibromide ND 4-Bromotlu010ben7ene 120 <br /> water and vapor samples are reported in ug/L soil and sludge samples in ug/kg wipes in ugN ipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water sampies 1 0 ug/L vapoi samples 0 5 ug/1- solid and sludge samples 5 0 ug/kg wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit NIA mean%analyte not applicable to this analysis <br /> (b) 2-pwpanone or dimethyl ketone (c) (2-chloroethoxy) ethcnc. (d) 2 I1LCanone (e) dichloromethane (t) 2 butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen Is present (r) liquid sample that contains greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content (k)peaks presuit rn this carbon range do not match the pattem of our standard for <br /> this analyte (1)methylbenzene (m)acetic acid ethenyl ester (n)Ltloroe thene (o)dimethylhenzutes <br /> DHS Certification No 1644 //>/ Edward Hamilton, Lab Director <br />