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Alpha Analytical, Inc. <br /> •f Q 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775) 355-1044• (775)355-0406 FAX• 1-800-283-1183 <br /> Date Work Order <br /> err-03 QC Summary Report W03091741 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B-DI <br /> File ID C IHPCHEM%MS111DATA10309lnO309l703 D Batch ID 8531 Analysts Date 09/17/2003 08 31 <br /> Sample ID MBLK-8531 Units pg1L Run ID GCIMSD_11_030917A Prep Date 0911712003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLtmit Highl-imit RPD Ref Val %RPD Qual <br /> Methanol NO 5000 <br /> Ethanol ND 5000 <br /> Surr Hexafluoro-2-propanol 417 500 83 69 135 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B-DI <br /> File ID C 1HPCHEM1MS1IWATA1030917103091704 D Batch ID 8531 Analysts Date 09/17/2003 09 07 <br /> Sample ID LCS-8531 Units 1i91L Run ID GCIMSD_'11_030917A Prep Date 09117/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> Methanol 242 5000 250 97 51 161 <br /> Ethanol 378 5000 50 76 47 137 <br /> Surr Hexafluoro-2-propanol 430 500 86 69 135 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW826013-13I <br /> File ]D C IHPCHEM1MS111DATA103091710309l706 D Batch ID 8531 Analysis Date 09/17/2003 10 15 <br /> Sample ID 03091120-01AMS Units pg/L Run ID GC/MSD_11_030917A Prep Date 09117/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLtmit HighLimit RPD Ref Val %RPD Qual <br /> Methanol 241 50 250 0 96 51 161 <br /> Ethanol 379 5 50 0 76 47 137 <br /> Surr Hexafluoro-2-propanol 445 500 89 69 135 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B-DI <br /> File ID C 1HPCHEM1MS1i1DATA1030917403091707 D Batch ID 8531 Analysis Date 09/17/2003 10 32 <br /> *ple ID 03091120-01AMSD Units tigIL Run ID GC/MSD_11_030917A Prep Date 09117/2003 <br /> Iyte Result PQL SpkVal SpkRefVal %REC LowLtmit Highl-imit RPD Ref Val %RPD Qua] <br /> Methanol 271 50 250 0 108 51 161 241 116 <br /> Ethanol 426 5 50 0 85 47 137 37 93 116 <br /> Surr Hexafluoro-2-propanol 428 500 86 69 135 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per liter,per client request <br />