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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 (775)355-1044•(775)355-0406 FAX • 1-800-283-1183 Bate Work Order Sep-03 OC Summary Report 03091741 Method Blank Type MBLK Test Code EPA Method SW8015 File ID Batch ID 8551 Analysis Date 09/19/2003 16 25 Sample ID MBLK_8551 Units Ng1L Run ID GCIFID_1_030919A Prep Date 0911912003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imd Hight.imit RPD Ref Val %RPD Qual TPH-E(Diesel) ND 50 Surr Nonane 86800 100000 87 40 135 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID Batch ID 8551 Analysis Date 09/19/2003 16 56 Sample ID LCS_8551 Units NgIL Run ID GCIFID_1_030919A Prep Date 0911912003 Analyte Result PQL SpkVa! SpkRefVal %REC LowLimit Hight-imt RPD Ref Val %RPD Qual TPH-E(Diesel) 2870 500 2500 115 57 135 Surr Nonane 105000 100000 105 40 135 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID Batch ID 8551 Analysis Date 09/1912003 17 58 Sample ID 03091840-01AMS Units NgIL Run ID GCIFID_1_030919A Prep Date 09119/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLrmit RPD Ref Val %RPD Qual TPH-E(Diesel) 3060 500 2500 4094 106 57 135 Surr Nonane 103000 100000 103 40 135 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID Batch ID 8551 Analysis Date 09/19/2003 19 00 Sample ID 03091840-01AMSD Units NgIL Run ID GCIFID_1-030919A Prep Date 09119/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Hight-imit RPD Ref Val %RPD Qua] TPH-E(Diesel) 3290 500 2500 4094 115 57 135 3060 725 r Nonane 88300 100000 88 40 135 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per liter,per client request