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Alpha Analytical, Inc. <br /> 255 Glendale Ave • Sutte 21 •Sparks,Nevada 84431-5778 <br /> (775) 355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Date Work Order <br /> _Sep-03 OC Summary Report 03091741 <br /> Method Blank. Type MBLK Test Code EPA Method SW8015B1DHS LOFT Manual <br /> File ID D 1HPCHEMIMS081DATA1030919103091906 D Batch ID MSBW0919B Analysis Date 09119/2003 12 19 <br /> Sample ID MBLK MS8W0919B Units pg1L Run 1D GCIMSD_8_030919A Prep Date 09119/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qua] <br /> TPH Purqeable ND 50 <br /> Surr 1,2-Dichlorcethane-d4 988 10 99 72 126 <br /> Surr Toluene-d8 105 10 105 71 128 <br /> Surr 4-Bromofluorobenzene 9 9 10 99 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8015B1DHS LUFT Manual <br /> File ID D IHPCHEMIMS081DATA1030919103091903 D Batch ID MS8W0919B Analysis Date 09/19/2003 11 10 <br /> Sample ID GLCS MS8W0919B Units pglL Run 1D GC/MSD_B 030919A Prep Date 09/1912003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 368 50 400 92 58 136 <br /> Surr 1,2-Dich]oroethane-d4 949 10 95 72 126 <br /> Surr Toluene-d8 10 4 10 104 71 128 <br /> Surr 4-Bromofluorobenzene 961 10 96 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8015BIDHS LUFT Manual <br /> File ID D 1HPCHEM IMS081DATA1030919103091911 D Batch ID MSSW0919B Analysis Date 09119/2003 14 16 <br /> Sample ID 03091741-01AGS Units pg1L Run ID GCIMSD_8_030919A Prep Date 09/1912003 <br /> Analyte result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 2070 250 2000 0 104 58 136 <br /> Surr 1,2-Dichloroethane-d4 484 50 97 72 126 <br /> Surr Toluene-de 514 50 103 71 128 <br /> Surr 4-Bromofluorobenzene 475 50 95 76 121 <br /> 1pie <br /> Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015BIDHS LOFT Manual <br /> D D IHPCHEMIMSOBIDATA1030922103092209 D Batch ID MS8W0919B Analysis Date 09122/2003 13 24 <br /> Sample ID 03091741-01AGSDR Units pg1L Run ID GCIMSD_8_030919A Prep Date 09122/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 1840 250 2000 0 92 58 136 2071 117 <br /> Surr 1,2-Dichloroethane-d4 486 50 97 72 126 <br /> Surr Toluene-d8 51 5 50 103 71 128 <br /> Surr 4-Bromofluorobenzene 474 50 95 76 121 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per liter,per client request <br />