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Report Date 05-May-1998 15 : 06 Page 3 :A SPL Houston Labs INITIAL CALIBRATION DATA p art Cal Date 01-MAY-1998 14 : 14 d' Cal Date 01-MAY-1998 16 : 04 Quant Method ISTD Origin Disabled T;_,eget Version 3 . 40 .;':.-egrator HP RTE Method file /var/chem/n. i/n980501 .b/n8260wL.m -al Date 05-May-1998 15 : 06 jimmy . t-ve Type Average 25.000 1 100-000 1 250.000 1 500.000 11000.000 1 _{Compound 1 Level 1 1 Level 2 1 Level 3 1 Level 4 1 Level 5 1 RRF 1 "s RSD 1 ---------------- 67 1,4-Dichlorobenzene 1 1.56114' 1.502021 1.545761 1.458731 1-430501 1.499631 3.7081 � .:]68 p-Isopropyltoluene 1 2.368681 2.493491 2.513871 2.430501 2.270341 2.415381 4.1011 69 1,2-Dichlorobenzene 1 1.208161 1.412191 1.407321 1.424801 1.407511 1.372001 6 6961 70 n-Butylbenzene 1 2.427211 2.673091 2.744111 2.696671 2.668491 2.641791 4.6801 71 1,2-Dibromo-3-Chloropropane 1 +++++ 1 0.085761 0.123581 D.132161 0.132161 0.118411 18.7001 72 1,2,4-Trichlorobenzene 1 0.494461 0,642571 0.703911 0.718351 0.689121 0.649681 14.0561 173 Naphthalene 1 1.323821 1.544191 1.761751 1,808831 1.720721 1.631861 12.2D51 74 Hexachlorobutadiene 1 0.349991 0.342751 0.361391 0.358041 0.321511 0.346741 4.5721 2,3-Trichlorobenzene 1 0.424561 0.530841 0.553721 0.524051 0.453201 0.497281 11.1331 cetonitrile 1 0.117641 0.080981 0.062471 0.046661 0.037141 0.06898 1 46.2221 j !:- i77 Acrylonitrile 1 0.119511 0.111191 0.102551 0.086501 0.070961 0.098141 19.8661 1 78 Allyl Chloride I D.384921 0-411371 0.362401 0.289981 0.261951 0.342121 18.5921 80 1,4-Dioxane I 0.003001 0.003841 0,004101 0,004641 0,004151 0.003951 15.2461 81 Ethyl Cyanide I 0.0B0001 0.083961 0.079291 0.074661 0.072221 0.078021 5.9371 -x'82 Ethyl Methacrylate 1 0.577341 0.609091 0.641281 0.628191 0.658411 0.622861 5.0091 83 Ethyl Ether 1 0.229651 0.235141 0.187591 0.149131 0.131101 0.186521 24.9971 ISI-,j 84 lodomethane 1 0.696101 0.656821 0.565821 0.408131 0.346691 0.534711 28-5621 i1. 85 Iso-Butyl Alcohol 1 0.013261 0.017271 0.017421 0.019671 0.023611 0.018251 20,7571 86 Methacrylonitrile 1 0.412891 0.526351 0-567031 0-619361 0-655961 0.556321 16.9311 fl7 Methyl Methacrylate 1 0.341731 0.405631 0.395401 0.391091 0.422881 0.391341 7.7471 88 trans-1,4-Dichloro-2-Butene I 0.325951 0.360771 0.313551 0.298131 0.275341 0.314751 10.14D1 89 Methyl t-8utyl Ether 1 1.283001 1.300411 1.327601 1,205151 1.126681 1.248571 6.5631 90 Butadiene 1 1.068271 0.546971 0.373611 0.227971 0.168531 0.477071 75.7481 zi92 Cyclohexane 1 0.925321 0.883731 0.929991 0.874561 0.962351 0.995171 3.4191 93 Dicyclopentadiene 1 3.848701 3.994521 3.926451 3.725581 3.457231 3.790491 5.5771 94 Hexane I 0.599691 0.614201 0.668051 0.622991 0.598991 0.620781 4.5581 95 t-Butyl Alcohol 1 0.197061 0.184891 0.191791 0.184161 0.177911 0.187161 3.9551 97 Acrolein 1 0.097451 0.098621 0.077301 0.061951 0.051661 0.075401 24,8951 1 � 9a 2,2,4-Trimethylpentane 1 1.050801 0.944011 0.906971 0.859561 0.803711 0.912811 10.2321 l � 1 195 2-Nitropropane 1 0.146951 0.176561 0.181521 0.171501 0.177241 0.170751 8.0671 i� I