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1 <br /> Report Date 05-May-1998 15 : 06 Page 4 <br /> f <br /> SPL Houston Labs <br /> INITIAL CALIBRATION DATA <br /> Start Cal Date 01-MAY-1998 14 : 14 <br /> End Cal Date 01-MAY-1998 16 : 04 <br /> Quant Method ISTD � ? <br /> Origin Disabled <br /> Target Version 3 . 40 <br /> Integrator HP RTE i ✓ <br /> Method file /var/chem/n. i/n980501 .b/n8260wL.m <br /> Cal Date 05-May-1998 15 : 06 jimmy <br /> curve Type Average <br /> 1 25.000 1 100.000 1 250.000 1 500.000 11000.000 <br /> Compound I Level 1 1 Level 2 1 Level 3 1 Level 4 1 Level 5 1 RRF I % RSD <br /> if <br /> 198 Ethyl Acetate 1 0.536131 0.562951 0.542521 0.517711 0.498111 0.531481 4.6441 <br /> 199 Cyclohexanone 1 0.004041 0.005671 0.005981 0.006821 0.006581 0.005821 18.7941 f.:f <br /> 200 1,1,2-Trichlorotrifluoroethanl 0.385101 0.386251 0.316121 0.254191 0.214731 0.311281 24.7151 �c <br /> 201 Ethylene Oxide 1 0.067791 0.061851 0.048021 0.037161 0.033821 0.049731 29.947 <br /> j 203 n-Butanol 1 0.007061 0.009691 0.0144BI 0.015051 0.015391 0.012331 30.3581 _ <br /> j 204 Di-Iso ro 1 Ether <br /> P PY 1 2.100681 2.039971 2.107001 1,974411 1.858231 2.016061 5-1221 <br /> 206 Cert-Amyl Methyl Ether 1 1.569501 1.390161 1.431661 1.325741 1.343731 1.412161 6.8811 _. <br /> j 207 Chlorotrifluoromethane 5.626851 3.081391 2.560451 1.884581 1.303071 2.931271 59.8011 <br /> 208 Ethyl t-Butyl Ether 1 1.945571 1.855201 1.917861 1.864641 1.779121 1.872481 3.42BI - -- <br /> $ 21 1,2-Dichloroethane-d4 1 0.062171 0.073191 0 07252 0.076991 0.072771 0,071531 7.7441 <br /> $ 36 Toluene-d8 1 1.240651 1.311471 1.304421 1,361161 1.326901 1.308921 3.3611 <br /> 1$ 56 Bromofluorobenzene I 0.558741 0.646911 0.643731 0.605341 0.572241 0.605391 6.6421 <br /> r ra <br /> }'J <br /> J..1 <br /> I <br /> r�7 f <br /> 4 % <br />