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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-36837-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: LCSD 720-97058/6 Client Sample ID: Lab Control Sample Dup <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 97058 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,2-Dichloroethane25.0 23.3 ug/L 93 70-126 3 20 <br /> Trichloroethene 25.0 24.4 ug/L 98 70-130 2 20 <br /> 1,2-Dichloropropane 25.0 24.6 ug/L 98 70-130 0 20 <br /> Dichlorobromomethane 25.0 26.3 ug/L 105 70-130 0 20 <br /> trans-1,3-Dichloropropene 25.0 25.9 ug/L 104 83-140 3 20 <br /> cis-1,3-Dichloropropene 25.0 26.2 ug/L 105 88-137 2 20 <br /> 1,1,2-Trichloroethane 25.0 24.9 ug/L 100 82.128 2 20 <br /> Tetrachloroethene 25.0 24.8 ug/L 99 70.130 1 20 <br /> Chlorodibromomethane 25.0 26.4 ug/L 106 78.145 3 20 <br /> Chlorobenzene 25.0 25.4 ug/L 102 70.130 0 20 <br /> Bromoform 25.0 26.4 ug/L 106 68.136 3 20 <br /> 1,1,2,2-Tetrachloroethane 25.0 26.6 ug/L 106 70.130 4 20 <br /> 1,3-Dichlorobenzene 25.0 26.0 ug/L 104 70-130 1 20 <br /> 1,4-Dichlorobenzene 25.0 25.4 ug/L 102 87.118 0 20 <br /> 1,2-Dichlorobenzene 25.0 25.6 ug/L 102 70-130 0 20 <br /> Chloromethane 25.0 22.0 ug/L 88 52.175 5 20 <br /> Bromomethane 25.0 23.8 ug/L 95 43-151 4 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 24.1 ug/L 96 42.162 1 20 <br /> ne <br /> EDB 25.0 25.9 ug/L 104 70-130 3 20 <br /> 1,2,4-Trichlorobenzene 25.0 25.7 ug/L 103 70-130 0 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 99 70.130 <br /> 4-Bromofluorobenzene 97 67.130 <br /> 1,2-Dichloroethane-d4(Surr) 93 67-130 <br /> Lab Sample ID: 720-36837-15 MS Client Sample ID: RPS-1 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch:97058 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1-Dichloroethene ND 25.0 22.2 ug/L 89 60.140 <br /> 1,1-Dichloroethane ND 25.0 23.9 ug/L 96 60.140 <br /> Dichlorodifluoromethane ND 25.0 18.8 ug/L 75 38.140 <br /> Vinyl chloride ND 25.0 21.2 ug/L 85 58-140 <br /> Chloroethane ND 25.0 22.4 ug/L 90 51-140 <br /> Trichlorofluoromethane ND 25.0 22.2 ug/L 89 60-140 <br /> Methylene Chloride ND 25.0 23.9 ug/L 96 40-140 <br /> trans-1,2-Dichloroethene ND 25.0 21.2 ug/L 84 60-140 <br /> cis-1,2-Dichloroethene 4.4 25.0 32.2 ug/L 111 60-140 <br /> Chloroform ND 25.0 24.0 ug/L 96 60-140 <br /> 1,1,1-Trichloroethane ND 25.0 24.6 ug/L 98 60-140 <br /> Carbon tetrachloride ND 25.0 24.5 ug/L 98 60-140 <br /> 1,2-Dichloroethane ND 25.0 23.5 ug/L 94 60.140 <br /> Trichloroethene 1.7 25.0 25.3 ug/L 94 60.140 <br /> 1,2-Dichloropropane ND 25.0 24.7 ug/L 99 60.140 <br /> Dichlorobromomethane ND 25.0 25.6 ug/L 102 60.140 <br /> trans-1,3-Dichloropropene ND 25.0 25.9 ug/L 104 60-140 <br /> cis-1,3-Dichloropropene ND 25.0 26.3 ug/L 105 60-140 <br /> TestAmerica San Francisco <br /> Page 25 of 49 08/23/2011 <br />