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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-36837-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID:720-36837-15 MS Client Sample ID: RPS-1 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 97058 L <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D 0/6 Rec Limits <br /> 1,1,2-Trichloroethane ND 25.0 24.9 ug/L 100 60-140 <br /> Tetrachloroethene ND 25.0 24.1 ug/L 96 60-140 <br /> Chlorodibromomethane ND 25.0 26.7 ug/L 107 60-140 <br /> Chlorobenzene ND 25.0 24.5 ug/L 98 60-140 <br /> Bromoform ND 25.0 24.9 ug/L 100 56-140 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 26.6 ug/L 106 60-140 <br /> 1,3-Dichlorobenzene ND 25.0 26.0 ug/L 104 60-140 F <br /> 1,4-Dichlorobenzene ND 25.0 25.3 ug/L 101 60-140 <br /> 1,2-Dichlorobenzene ND 25.0 25.4 ug/L 102 60-140 <br /> Chloromethane ND 25.0 20.7 ug/L 83 52-140 <br /> Bromomethane ND 25.0 21.9 ug/L 88 23-140 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 23.1 ug/L 92 60-140 <br /> ne <br /> EDB ND 25.0 25.9 ug/L 104 60-140 <br /> 1,2,4-Trichlorobenzene ND 25.0 25.0 ug/L 100 60-140 <br /> MS MS El <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surf) 98 70-130 <br /> 4-Bromofluorobenzene 95 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 94 67-130 <br /> Lab Sample ID: 720-36837-15 MSD Client Sample ID: RPS-1 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch:97058 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene ND 25.0 23.1 ug/L 92 60-140 4 20 <br /> 1,1-Dichloroethane ND 25.0 24.3 ug/L 97 60-140 2 20 <br /> Dichlorodifluoromethane ND 25.0 19.1 ug/L 76 38-140 2 20 <br /> Vinyl chloride ND 25.0 22.3 ug/L 89 58-140 5 20 <br /> Chloroethane ND 25.0 23.6 ug/L 94 51-140 5 20 <br /> Trichlorofluoromethane ND 25.0 22.0 ug/L 88 60-140 1 20 <br /> Methylene Chloride ND 25.0 23.9 ug/L 96 40-140 0 20 <br /> trans-1,2-Dichloroethene ND 25.0 21.7 ug/L 86 60-140 2 20 <br /> cis-1,2-Dichloroethene 4.4 25.0 32.2 ug/L 111 60-140 0 20 <br /> Chloroform ND 25.0 23.9 ug/L 96 60-140 0 20 <br /> 1,1,1-Trichloroethane ND 25.0 24.7 ug/L 99 60-140 0 20 <br /> Carbon tetrachloride ND 25.0 24.6 ug/L 98 60-140 0 20 <br /> 1,2-Dichloroethane ND 25.0 22.5 ug/L 90 60-140 4 20 <br /> Trichloroethene 1.7 25.0 25.3 ug/L 94 60-140 0 20 <br /> 1,2-Dichloropropane ND 25.0 24.5 ug/L 98 60-140 1 20 <br /> Dichlorobromomethane ND 25.0 25.6 ug/L 102 60-140 0 20 <br /> trans-1,3-Dichloropropene ND 25.0 25.1 ug/L 100 60-140 3 20 <br /> cis-1,3-Dichloropropene ND 25.0 25.9 ug/L 104 60-140 2 20 <br /> 1,1,2-Trichloroethane ND 25.0 24.3 ug/L 97 60-140 2 20 <br /> Tetrachloroethene ND 25.0 23.9 ug/L 96 60-140 1 20 <br /> Chlorodibromomethane ND 25.0 25.8 ug/L 103 60-140 3 20 <br /> Chlorobenzene ND 25.0 25.3 ug/L 101 60-140 3 20 <br /> Bromoform ND 25.0 24.9 ug/L 100 56-140 0 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 26.3 ug/L 105 60-140 1 20 <br /> TestAmerica San Francisco <br /> Page 26 of 49 08/23/2011 <br />