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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-56569-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 524.2 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: 720-56569-1 MS Client Sample ID: 7501 KIERNAN 2008 EFF <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 174537 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Dibromochloromethane ND 10.0 7.59 ug/L 76 70-130 <br /> Methylene Chloride ND 10.0 8.58 ug/L 86 70-130 <br /> Tetrachloroethene ND 10.0 7.43 ug/L 74 70-130 <br /> trans-l,2-Dichloroethene ND 10.0 8.58 ug/L 86 70-130 <br /> trans-1,3-Dichloropropene ND 10.0 8.13 ug/L 81 70-130 <br /> Trichloroethene ND 10.0 7.73 ug/L 77 70-130 <br /> Trichlorofluoromethane ND 10.0 8.62 ug/L 86 70-130 <br /> Vinyl chloride ND 10.0 9.62 ug/L 96 70-130 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichlorobenzene-d4 90 70-130 <br /> 4-Bromofluorobenzene(Surr) 97 70-130 <br /> Lab Sample ID: 720-56569-1 MSD Client Sample ID: 7501 KIERNAN 2008 EFF <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 174537 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,1-Trichloroethane ND 10.0 8.05 ug/L 80 70-130 2 20 <br /> 1,1,2,2-Tetrachloroethane ND 10.0 8.60 ug/L 86 70-130 6 20 <br /> 1,1,2-Trichloroethane ND 10.0 8.23 ug/L 82 70-130 4 20 <br /> 1,1-Dichloroethane ND 10.0 8.57 ug/L 86 70-130 2 20 <br /> 1,1-Dichloroethene ND 10.0 8.59 ug/L 86 70-130 3 20 <br /> 1,2-Dibromoethane(EDB) ND 10.0 8.07 ug/L 81 70-130 4 20 <br /> 1,2-Dichlorobenzene ND 10.0 7.03 ug/L 70 70-130 2 20 <br /> 1,2-Dichloroethane ND 10.0 8.07 ug/L 81 70-130 3 20 <br /> 1,2-Dichloropropane ND 10.0 8.58 ug/L 86 70-130 2 20 <br /> 1,3-Dichlorobenzene ND 10.0 7.29 ug/L 73 70-130 2 20 <br /> Bromodichloromethane ND 10.0 8.45 ug/L 85 70-130 2 20 <br /> Bromoform ND 10.0 8.00 ug/L 80 70-130 6 20 <br /> Bromomethane ND 10.0 10.6 ug/L 106 70-130 2 20 <br /> Carbon tetrachloride ND 10.0 7.88 ug/L 79 70-130 0 20 <br /> Chlorobenzene ND 10.0 8.83 ug/L 88 70-130 3 20 <br /> Chloroethane ND 10.0 9.84 ug/L 98 70-130 5 20 <br /> Chloroform ND 10.0 8.33 ug/L 83 70-130 1 20 <br /> Chloromethane ND 10.0 10.3 ug/L 103 70-130 6 20 <br /> cis-1,2-Dichloroethene ND 10.0 7.98 ug/L 80 70-130 2 20 <br /> cis-1,3-Dichloropropene ND 10.0 9.04 ug/L 90 70-130 5 20 <br /> Dibromochloromethane ND 10.0 7.85 ug/L 78 70-130 3 20 <br /> Methylene Chloride ND 10.0 8.72 ug/L 87 70-130 2 20 <br /> Tetrachloroethene ND 10.0 7.56 ug/L 76 70-130 2 20 <br /> trans-1,2-Dichloroethene ND 10.0 8.49 ug/L 85 70-130 1 20 <br /> trans-1,3-Dichloropropene ND 10.0 8.56 ug/L 86 70-130 5 20 <br /> Trichloroethene ND 10.0 7.80 ug/L 78 70-130 1 20 <br /> Trichlorofluoromethane ND 10.0 8.84 ug/L 88 70-130 3 20 <br /> Vinyl chloride ND 10.0 9.92 ug/L 99 70-130 3 20 <br /> TestAmerica Pleasanton <br /> Page 18 of 29 4/10/2014 <br />