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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-56569-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 524.2 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: 720-56569-1 MSD Client Sample ID: 7501 KIERNAN 2008 EFF <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 174537 L <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichlorobenzene-d4 91 70-130 <br /> 4-Bromofluorobenzene(Surr) 98 70-130 <br /> Method: 300.0 -Anions, Ion Chromatography F <br /> Lab Sample ID: MB 720-156705/4 Client Sample ID: Method Blank F <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 156705 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Nitrate as N ND 0.23 mg/L 04/04/14 12:47 1 <br /> Lab Sample ID: LCS 720-156705/5 Client Sample ID: Lab Control Sample <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 156705 El <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 2.26 2.17 mg/L 96 90-110 <br /> Lab Sample ID: 720-56569-6 MS Client Sample ID: 5725 HALL 2009 INF <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 156705 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 5.7 22.6 27.3 mg/L 95 80-120 <br /> Lab Sample ID: 720-56569-6 MSD Client Sample ID: 5725 HALL 2009 INF <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 156705 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Nitrate as N 5.7 22.6 27.3 mg/L 95 80-120 0 20 <br /> TestAmerica Pleasanton <br /> Page 19 of 29 4/10/2014 <br />