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N 10 2nd Arra //lh,PD7,Pacheco.CA 94553-5560 T. McCampbell Analyti nc. Telephone "+ 798-1620 Fax:925-798-1622 http://www.iuccam;ibell.com E-mail:main{<emccamphell.cam Ground Zero Analysis, Inc. Client Project ID: #479; Kooyman Date Sampled: 10/01/02 1714 Main Street Date Received: 10/03/02 )tiscalon, CA 95320 Client Contact: Greg Stahl Date Extracted: 10/03/02 -_LClientP.O.: Date Analyzed: 10/04/02 Semi-Volatile Organics by GC/MS(Basic Target List)* Extraction Method: SW3550C Analytical Mediod: SW8270D Work Order:0210071 Lab ID 0210071-001 A Client JD j --- KSD-3 -- --- Matrix - Soil R nin Compound Concentration * DF `c°°�;,E Compound Concentration * DF A m;;s Acenaphthene ND<33 100 0.33 Acenaphthylene ND<33 100 _0.33 Anthracene ND<33 100 0.33 Benzidine ND<l60 100 1.6 .Benz-oic Acid ND<l60 100 1.6 ! Benz(a)anthracene ND<33 100 0.33 Benz (b)fluoranthene ND<33 100 0.33 Benzo(k)fluoranthene ND<33 100 0.33 Benzo(g,h,i)peryicne ND<33 100 0.33 Benzo(a)pyrenc ND<33 100 0.33 Benzyl Alcohol _ ND<66 100 0.66 Bis(2-chloroethoxy)Methane ND<33 100 0.33 Bis(2-chloroethyl)Ether -- - ND<33 T 100 0.33 Bis_(2-chloroisopropyl)Ether ND<33_ _ 100 0.33 Bis(2-ethylhexyl)Phthalate ND<33 100 0.33 4-Bromophenyl Phenyl Ether _ ND<33 - 100 0.33 Buiylbenzyi Phthalate ND<33 100 0.33 4-Chloroaniline ND<66 100 0.66 4-Chloro-3-methylphenol ND<33 100 0.33 2-Chloronaphthalene ND<33 100 0.33 2-Chlorophenol ND<33 100 0.33 4-Chlorophenyl Phenyl Ether ND<33 100 0.33 -i Chrysene ND<33 - 100 0.33 Dibenzo(a,h)anthracene ND<33 100 0.33 Dibenzofuran ND<33 100 j 0.33 Di-n-butyl Phthalate ND<33 100 0.33 -- - -- 1,2-Dichlorobenzene ND<33 100 0.33 1,3-Dichlorobenzene ND<33 too 0.33 1,4-1)ichlorobenzene ND<33 100 0.33 3,3-Dichlorobenzidine ND<66 100 0.66 2,4-_Dich_lorophe not ND<33 ! 100 0.33 Diethyl Phthalate ND<33 100 0.33 2,4-Dimeth l henol _ _ ND<33 100 1 0.33 Dimethyl Phthalate ND<33 100 0.33 4,6-Dinitro-2-methyl_pheno_l ND<160 100 ' 1.6 2,4-Dinitrophenol ND<160 100 1.6 2,4-Dinitrotoluene ND<33 100 1 0.33 2,6-_Dinitrotoluene ND<33 100 _0.33 Di-n-octyl Phthalate ND<33 100 0.33 1,2-Diphenylhyd7-azine ND<33 100 0.33 Fluoranthene ND<33 100 0.33 Fluorene ND<33 100 0.33 H_exachlorobenzene ND<33 100 0.33 HexachIorobutadiene _ ND<33 t00 0.33 Hex ac hlorocyclopentadiene ND<160 100 1.6 Hexachloroethane ND<33 100 0.33 ]adeno(1,2,3-cd)pyrene ND<33 100 0.33 lsophorone ND<33 100 0.33 2-Methylnaphthalene ND<33 100 0.33 . 2-M_ethylphenol(o-Cresol) ND<33 100 0.33 3&/or 4-Methylphenol(m,p-Cresol) ND<33 100 0.33 Naphthalene ND<33 140 0.33 2-Nitroaniline ND<160 100 1.6 3-Nitroaniline ND<160 100 1.6 4-Nitroaniline N13<1 60 100 1.6 2-Nitrophenol ND<160 100 1.6 _4-Nitrophenol _ND<160 WO1.G�Nitrobenzene ND<33 100 0.33 N-Nitrosodiphenylamine �- ND<33 100 0.33 N-Nitrosodi-n-propylamine ND<33 100 0.33 Pentachlorophenol ND<160 100 1.6 Phenanthrene ND<33 100 0.33 Phcnol ND<33 100 0.33' Pyrene ND<33 100 0.33 11214-Trichlorobenzene - _ ND<33 100 0.33 2,4,5-Trichlorophenol ND<33 - 100 0.33 2.4,6-Trichlorophenol ND<33 100 0.33 Surrogate Recoveries(%) %SSL ---# %SS2: ---# %SS3: 97.6 LL %SS4: 102 %SS6: 90.1 Comments:j *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in mg/kg, wipe samples in ug/wipe, product/oil/non-aqueous liquid samples in mg/L. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. #)sunogate diluted out of range;&)low or no surrogate due to matrix interference. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high organic content. DHS Certification No. 1644 Edward Hamilton,Lab Director