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t' Analytical <br /> 7 110 2nd Avenue South.11D7.Pacheco,CA 04553-5560 <br /> L�o McCampbell Analytical Inc. Telephone:925-798-3620 Fax:925-796-1622 <br /> Ifttp:llwww,mccampbcll.com E-nail:mam(ci!mccatnpbell.com <br /> Ground Zero Analysis, Inc. Client Project ID: #479;Kooyman Date Sampled: 10/01/02 <br /> 1714 Main Street Date Received: 10/03/02 <br /> Escalon, CA 95320 Client Contact: Greg Stahl Date Extracted: 10/03/02 <br /> [Client P.O.: Date Analyzed: 10/04/02-10108102 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0210071-00 I A Reporting Limit for DF=1: <br /> - ND means not detected <br /> Client ID KSD1-3 above the re ortiny limit <br /> Matrix S <br /> Extraction Type TTLC TTLC(mglKb) mg!L <br /> ICP Metals,Concentration* <br /> Analvtical Method:6010C Extraction Method: SW3050B Work Order:0210071 <br /> Dilution Factor ] ' 1 1 <br /> Antimony ND + 2.5 NA <br /> ti - ---- — <br /> Barium 280 --- - - - ---- <br /> 2-5 NA <br /> Beryllium ND 0.5 NA <br /> Cadmium - -- 1.7 _- 0.5 NA <br /> Chromium 27 0.5 NA <br /> Cobalt -------_- _ 4.3 _ - --- - _2.0 __—__NA- _- <br /> �Copper � 370 V _ 2.0 NA <br /> Lead - -- ----- 25 3.0 ------NA <br /> Molybdenum — — - - ND — 2.0 NA- <br /> Nickel 15 -- - 2.0 -- --- NA <br /> Silver ND 1.0 NA <br /> Vanadium 49 2.0 NA <br /> zine 1600 1.0 NA <br /> %SS: 105 - -- -- <br /> GFAA Metals,Concentration* <br /> Analytical Method:SW7010 Extraction Method:SW3050B <br /> Dilution Factor l 1 1 <br /> Arsenic 2.5 2.5 NA <br /> Selenium ND 2.5 NA <br /> Thallium ND 2.5 NA <br /> Cold Vapor Metals,Concentration* <br /> Analvtical Method:SW7471B Extraction Method: SAV7471B <br /> _ _ Dilution Factor 1 _ 1 _ 1 <br /> Mercury I 0.51 I 0.06 NA <br /> I <br /> rComments ----- <br /> *water samples are reported in mg/L,soillsludge/solid/product samples in mg/kg,wipes in ug/wipe and all TCLP I STLC/DISTLC/SPLP extracts in <br /> mg/L. <br /> ND means not detected above the reporting limit;N/A means not applicable to this sample or instrument. <br /> Analytical Methods: EPA 6010C1200.7 for all elements except:200.9(water-Sb,As,Pb,Se,Tl);245.1 (Hg);7010(sludge/soil/solid/oillproduct/wipes- <br /> As,Se,TI);7471 B(Hg). <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the extraction fluid. <br /> DISTLC results are not applicable to STLC regulatory limits. <br /> i)liquid sample that contains greater than--2 vol.%sediment;this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations;z)reporting limit raised due to matrix interference. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />