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McCampbell Analytical nc. ][0 2nd Avenu .#D7,Pacheco.CA 94553-5560 i <br /> Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccampbclLcom E-mail:main©mccampb0l.com <br /> Ground Zero Analysis, Inc. Client Project ID: #479;Kooyman Date Sampled: ]0/01/02 <br /> E 1714 Main Street Date Received: 10/03/02 <br /> h <br /> i <br />€ Escalon, CA 95320 Client Contact, Greg Stahl Date Extracted: 10/18/02-10120/02 <br /> Client P.O.: Date Analyzed: 10/22/02 <br /> ICP Metals* <br /> =Xtr-ac1fionmethod: CA Title 22 Analytical methods: SW6010C <br /> Work Order. 0210071 <br /> Lab ID Client ID Matrix Extraction Copper DF %SS <br /> 0210071-001 A KSD1-3 S STLC 02.8 1 N/A <br /> I <br /> i <br /> Reporting Limit for DF=1; W TTLC NA mg/L <br /> ND means not detected at or <br /> above the reporting limit S STLC 0.05 mg/L <br /> "water samples are reported in mg/L,soillsludgelsolid/product samples in mg/kg,wipes in ug/wipe and all TCLP I STLC I DISTLC/SPLP extracts in <br /> mg/L. <br /> ND means not detected above the reporting limit;N/A means not applicable to this sample or instrument. <br /> Analytical Methods:EPA 6010C/200.7 for all elements except:200.9(water-Sb,As,Pb,Se,Tl);245.1 (Hg);7010(sludge/soil/solid/oil/product/wipes- <br /> As,Se,Ti);7471 B(Hg). <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the extraction fluid. <br /> DISTLC results are not applicable to STLC regulatory limits. i <br /> i <br /> i)liquid sample that contains greater than--2 vol.%sediment;this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations;z)reporting limit raised due to matrix interference. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />