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I,, y 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> ® pb <br /> MCCamell Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" I <br /> http://www.mccampbeLLcom/E-mad:nnnnOmccampbell.com <br /> Quality Control Report <br /> Client: Neil 0.Anderson&Associates WorkOrder: 1404047 <br /> Date Prepared: 4/4/14 BatchlD: 88975 <br /> Date Analyzed: 4/4/14 Extraction Method: SW3550B <br /> Instrument: GC21 Analytical Method: SW8270C <br /> Matrix: Soil Unit: mg/Kg <br /> Project: #LZ140001;NOA Drywell,Lodi,CA Sample ID: MBIL.CS-88975 <br /> 1404047-OOIAMS/MSD <br /> QC Summary Report for SW8270C <br /> Analyte MB LCS RL SPK MB LCS LCS <br /> Result Result Val SS%REC %REC Limits <br /> Di-n-octyl Phthalate ND - 0.50 - - - - <br /> 1,2-Diphenylhydrazine ND - 0.25 - - - - <br /> Fluoranthene ND - 0.25 - - - - <br /> Fluorene ND - 0.25 - - - - <br /> Hexachlorobenzene ND - 0.25 - - - - <br /> Hexachlorobutadiene ND - 0.25 - - - - <br /> Hexachlorocyclopentadiene ND - 1.3 - - - - <br /> Hexachloroethane ND - 0.25 - - - - <br /> Indeno(1,2,3-cd)pyrene ND - 0.25 - - - - <br /> Isophorone ND - 0.25 - - - - <br /> 2-Methylnaphthalene ND - 0.25 - - - - <br /> 2-Methylphenol(o-Cresol) ND - 0.25 - - - - <br /> 3 Wor 4-Methylphenol(m,p-Cresol) ND - 0.25 - - - - <br /> Naphthalene ND - 0.25 - - - - <br /> 2-Nitroaniline ND - 1.3 - - - <br /> 3-Nitroaniline ND - 1.3 - - - - <br /> 4-Nitroaniline ND - 1.3 - - - - <br /> Nitrobenzene ND - 0.25 - - - - <br /> 2-Nitrophenol ND - 1.3 - - - - <br /> 4-Nitrophenol ND 4.241 1.3 5 - 84.8 30-130 <br /> N-Nitrosodiphenylamine ND - 0.25 - - - - <br /> N-Nitrosodi-n-propylamine ND 4.508 0.25 5 - 90.2 30-130 <br /> Pentachlorophenol ND 4.478 1.3 5 - 39.6 30-130 <br /> Phenanthrene ND - 0.25 - - - - <br /> Phenol ND 5.516 0.25 5 - 110 30-130 <br /> Pyrene ND 5.098 0.25 5 - 102 30-130 <br /> 1,2,4-Trichlorobenzene ND 5.2 0.25 5 - 104 30-130 <br /> 2,4,5-Trichlorophenol ND - 0.25 - - - - <br /> 2,4,6-Tdchlorophenol ND - 0.25 - - - - <br /> Surrogate Recovery <br /> 2-Fluorophenol 4.266 4.999 5 85 100 30-130 <br /> Phenol-d5 4.248 5.111 5 85 102 30-130 <br /> Nitrobenzene-d5 3.622 4.419 5 72 88 30-130 <br /> 2-Fluorobiphenyl 3.74 4.321 5 75 86 30-130 <br /> 2,4,6-Tribromophenol 3.029 3.802 5 61 76 30-130 <br /> 4-Terpheny1d14 4.189 5.168 5 84 103 30-130 <br /> (Cont.) <br /> CDPH ELAP 1644♦NELAP 4033ORELAP " QA/QC Officer <br /> Page 52 of 78 <br />