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1534 Willow pass Road,Pinsbmg,CA 94565-1701 <br /> ® MCCampbell Anal cal, Inc.. Toll Free Telephone;(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" I <br /> nnp://w .mecanpbea.com/&mail:main@rne ampbelicom <br /> Quality Control Report <br /> Client: Neil O.Anderson&Associates WorkOrder: 1404047 <br /> Date Prepared: 4/4/14 BatchlD: 88975 <br /> Date Analyzed: 4/4/14 Extraction Method: SW3550B <br /> Instrument: GC21 Analytical Method: SW8270C <br /> Matrix: Soil Unit: mg/Kg <br /> Project: #LZ140001;NOA Drywell,Lodi,CA Sample ID: MB/LCS-88975 <br /> 1404047-OOIAMS/MSD <br /> QC Summary Report for SW8270C <br /> Analyte MS MSD SPK SPKRef MS MSD MSIMSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> Acenaphthene 4.582 4.551 5 ND 91.6 91 30-130 0.677 30 <br /> 4-Chloro-3-methylphenol 5.961 5.963 5 ND 119 119 30-130 0 30 <br /> 2-Chlorophenol 5.635 5.809 5 ND 113 116 30-130 3.04 30 <br /> 1,4-Dichlorobenzene 4.616 4.563 5 ND 92.3 91.3 30-130 1.16 30 <br /> 2,4-Dinitrotoluene 5.578 5.872 5 ND 112 117 30-130 5.13 30 <br /> 4-Nitrophenol 4.588 4.701 5 ND 91.8 94 30-130 2.43 30 <br /> N-Nitrosodi-n-propylamine 4.282 4.294 5 ND 85.7 85.9 30-130 0.270 30 <br /> Pentachlorophenol 5.488 5.264 5 ND 110 105 30-130 4.17 30 <br /> Phenol 5.36 5.5 5 ND 107 110 30-130 2.57 30 <br /> Pyrene 5.011 5.109 5 ND 100 102 30-130 1.93 30 <br /> 1,2,4-Tdchlorobenzene 5.578 5.173 5 ND 112 103 30-130 7.53 30 <br /> Surrogate Recovery <br /> 2-Fluorophenol 4.956 5.072 5 99 101 30-130 2.33 30 <br /> Phenol-d5 4.911 5.022 5 98 100 30-130 2.24 30 <br /> Nitrobenzene-d5 4.645 4.398 5 93 88 30-130 5.46 30 <br /> 2-Fluorobiphenyl 4.543 4.381 5 91 88 30-130 3.64 30 <br /> 2,4,6-Tdbromophenol 4.054 3.902 5 81 78 30-130 3.82 30 <br /> 4-Terphenyl-dl4 5.085 5.213 5 102 104 30-130 2.48 30 <br /> CDPH ELAP 16441NELAP 4033ORELAP " QA/QC Officer <br /> Page 53 of 78 <br />