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American Environmental Network WORK ORDER 9803361 QUALITY CONTROL REPORT PAGE QR-3 ' ANALYSIS. Metals Scan by ICP MATRIX Water ' METHOD BLANK SAMPLES ------ - - ------ -------- ----------------- SAMPLE TYPE Blank-Method/Media blank LAB ID IFW POW INSTR RUN ICP1980408175800/1/ - - ----------------- ----------- ------------- INSTRUMENT TJA Enviro 36 PREPARED --- BATCH ID IFW040798-F UNITS mg/L ANALYZED 04/08/98 DILUTION 1 000000 ' METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIM RPD (X) LIMIT (X) Ag Silver ND 0 005 Al Aluminum 0 0181(J) 0 1 Ba Barium NO 0 01 Be Beryllium ND 0 002 Ca Calcium ND 0 2 Cd Cadmium NO 0 005 Co Cobalt ND 0 005 Cr Chromium NO 0 01 Cu Copper NO 0 01 Fe Iron ND 0 1 K Potassium ND 0 1 ' Mg Magnesium NO 0 04 Mn Manganese NO 0 005 Mo Molybdenum NO 0 01 Na Sodium 0 1140) 0 5 Ni Nickel ND 0 01 ' Pb Lead NO 0 04 Sb Antimony NO 0 02 Tl Thallium ND 0 05 V Vanadium ND 0 005 Zn Zinc 0 0099(.3) 0 01 I* -------- --- --- -------------------------------------------------------- ------------------------------------------------- LABORATORY CONTROL SAMPLES SAMPLE-TYPE---'3ke-Method/Nediablank LAB-ID IFW LCO TNSTR RUN ICP1980408175800/3/1 INSTRUMENT T LEnviro 36 PREPARED — BATCH ID IFW040798-F ANALYZED 04/08/98 DILUTION 1 000000 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPO ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Ag Silver 0 0249 NO 0 005 0 0250 99 6 80 120 A? Aluminum 1 06 0 0181(J) 0 1 1 00 104 80 120 ' Ba Barium 1 01 NO 0 01 1 00 101 80 120 Be Beryllium 0 0280 NO 0 002 0 0250 112 80 120 Ca Calcium 10 2 NO 0 2 10 0 102 80 120 Cd Cadmium 0 0436 ND 0 005 0 0500 87 2 80 120 ' Co Cobalt 0 255 NO 0 005 0 250 102 80 120 Cr Chromium 0 0987 NO 0 01 0 100 98 7 80 120 Cu Copper 0 127 NO 0 01 0 125 102 80 120 Fe Iron 0 513 NO 0 1 0 500 103 80 120 K Potassium 9 86 ND 0 1 10 0 98 6 80 120 ' M9 Magnesium 10 1 NO 0 04 10 0 101 80 120 Mn Manganese 0 264 NO 0 005 0 250 106 80 120 Mo Molybdenum 0 202 NO 0 01 0 200 101 80 120 Na Sodium 10 2 0 114(J) 0 5 10 0 101 80 120 Ni N-.ckel 0 252 NO 0 01 0 250 101 80 120 Pb Lead 0 522 ND 0 04 0 500 104 80 120 Sb Antimony 0 477 NO 0 02 0 500 95 4 80 120 Tl Thallium 0 494 NO 0 05 0 500 98 8 80 120 V Vanadium 0 253 NO 0 005 0 250 101 80 120 ' Zn Zinc 0 245 0 0001U 25D------ ----- 80 120 - -- - ------- .............................. -- ----------- ........... PLE TYPE Spike-Method/Media blank LAB ID IFW_LCS INSTR RUN ICP1980408175800/2/1 STRUMENT TJA Enviro 36 PREPARED BATCH ID IFW040798-F ' ITS mg/L ANALYZED 04/08/98 DILUTION 1 000000 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Ag Sliver 0 0256 NO 0 005 0 0250 102 80 120