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American Environmental Network WORK ORDER- 9803361 QUALITY CONTROL REPORT PAGE QR-3 ' ANALYSIS. Metals Scan by ICP MATRIX Water ' METHOD BLANK SAMPLES ----- - -- ---- SAMPLE TYPE Blank-Method/Media blank LAB ID IFW PBW INSTR RUN ICP1980408175 -- -------------------------- - -•----------.-.--. ...--------------------..-__----------800/1/ -- --- INSTRUMENT TJA Enviro 36 PREPARED BATCH ID IFW040798-F UNITS mg/L ANALYZED 04/08/98 DILUTION 1 000000 ' METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Ag Silver ND 0 005 Al Aluminum 0 0181(J) 0 1 Ba Barium NO 0 01 Be Beryllium ND 0 002 Ca Calcium NO 0 2 Cd Cadmium ND 0 005 Co Cobalt NO 0 005 Cr Chromium NO 0 01 Cu Capper ND 0 01 Fe Iron NO 0 1 K Potassium ND 0 1 ' Mg Magnesium NO 0 04 Mn Manganese ND 0 005 Mo Molybdenum NO 0 01 Na Sodium 0 114(J) 0 5 Ni Nickel NO 0 01 ' Pb Lead ND 0 04 Sb Antimony ND 0 02 Ti Thallium NO 0 05 V Vanadium ND 0 005 Zn Zinc 0 0099(1) 0 01 M ----------- --- -- -------------------------------------- --------------- ------------------------- --------------------- LABORATORY CONTROL SAMPLES SAMPLE TYPE Spike-Method/Media blank LAS ID IFW LCD INSTR RUN ICP1980408175800/3/1 INSTRUMENT TJA Enviro 36 PREPARED BATCH ID IFW040798-F UNITS mg/L ANALYZED 04/08/98 DILUTION 1 000000 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPA ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (t) Ag Silver 0 0249 ND 0 005 0 0250 99 6 80 120 Al Aluminum 1 06 0 0181(J) 0 1 1 00 104 80 120 ' Ba Barium 1 01 ND 0 01 1 00 101 80 120 Be Beryllium 0 0280 NO 0 002 0 0250 112 80 120 Ca Calcium 10 2 ND 0 2 10 0 102 80 120 Cd Cadmium 0 0436 NO 0 005 0 0500 87 2 80 120 ' Co Cobalt 0 255 ND 0 005 0 250 102 80 120 Cr Chromium 0 0987 ND 0 01 0 100 98 7 80 120 Cu Co per 0 127 NO 0 01 0 125 102 80 120 Fe Iron 0 513 NO 0 1 0 500 103 80 120 K Potassium 9 86 NO 0 1 10 0 98 6 80 120 ' Mg Magnesium 10 1 ND 0 04 10 0 101 80 120 Mn Manganese 0 264 ND 0 005 0 250 106 80 120 No Molybdenum 0 202 NO 0 01 0 200 101 80 120 Na Sodium 10 2 0 1140) 0 5 10 0 101 80 120 Ni Nickel 0 252 NO 0 01 0 250 101 80 120 ' Pb Lead 0 522 ND 0 04 0 500 104 80 120 Sb Antimony 0 477 ND 0 02 0 500 95 4 80 120 Tl Thallium 0 494 ND 0 05 0 500 98 8 80 120 V Vanadium 0 253 NO 0 005 0 250 101 80 120 Zn Zinc 0 246 0 0099(j).......0 ---.. 0 250--------. 94 _.._.._80....120 - ........................... eAMPLE I ---TYPE Spike Method/Media blank LAB ID IFWLCS INSTR RUN ICP1980408175800/ 12/1 STRUMENT TJA Enviro 36 PREPARED BATCH ID IFW040798-F ITS mg/L ANALYZED 04/08/98 DILUTION 1 000000 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (Z) LOW HIGH RPD (X) LIMIT (X) Ag Silver 0 0256 NO 0 005 0 0250 102 80 120