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110 2nd Avenue South #D7,Pacheco,CA 94553-5560 <br /> F4 <br /> Campbell Analytical Inc <br /> McTelephone 925-796-1620 Fax 925-796-1622 <br /> h //www mcca bell corn E-mail_TE2arriccarnpbell com <br />' Advanced GeoEnvironmental, Inc Client Project ID Flame Liquors Date Sampled 03/04/03 <br /> • 837 Shaw Road Date Received 03/05/03 <br />' Client Contact Bill Little Date Extracted 03/06/03-03107103 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 03/06103-03/07103 <br /> IGasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline with BTEX and MTBE* <br /> Extraction method SW5030B Analytical methods SW8021B/8015Cm WorkOtder 0303039 <br />' Lab ID Client ID Matrix TPH(g) MTBE Benzene Toluene Ethylbenzene Xylenes DF %SS <br /> 001A M W 1/030403 W ND ND ND ND ND 1 101 <br />' 002A MW2/030403 W 340,a ___ 27 1 2 7 3 !0 1 108 <br /> 003A MW3/030403 W ND ND ND ND ND I 107 <br />' 004A MW4/030403 W ND ND ND ND ND l 103 <br /> 1 <br /> 1 <br /> Reportmg Limit for DF=1 `7y7 50 5 0 05 05 0 5 0 5 1 µg11 <br />' ND means not detected at or <br /> above the reporting limit S NA NA NA NA NA NA 1 mg/Kg <br /> "water and vapor samples are reported in gg/L,soil and sludge samples in mg/kg,wipe samples to gg/wipe,and TCLP extracts inµg/I <br />' #cluttered chromatogram,sample peak coelutes with surrogate peak <br /> +The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical 1s not responsible for their interpretation a) <br /> unmodlfled or weakly modified gasoline is significant,b)heavier gasoline range compounds are significant(aged gasoline?),c)lighter gasoline range <br />' compounds(the most mobile fraction)are significant,d)gasoline range compounds having broad chromatographic peaks are significant,biologically <br /> altered gasohnel,e)TP1-I pattern that does not appear to be derived from gasoline(stoddard solvent/mmcral spirlV),f)one to a few isolated non-target <br /> peaks present,g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible sheen/product is present,i)liquid <br /> sample that contains greater than--2 vol %sediment,I)reporting limit raised due to high MTBE content,k)TPH pattern that does not appear to be <br /> derived from gasoline(aviation gas) m)no recognizable pattern <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />