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110 2nd Avenue South ND7 Pacheco CA 94553-5560 <br /> ampbell Analytical Inc <br /> McCTelephone 925-798.1620 Fax 925-798-1622 <br />' h J/www mcc bel]com E-mail mautQrriccarmbell.corn <br /> • Advanced GeoEnvironmental,Inc Client Project ID Flame Liquors Date Sampled 03/04/03 <br /> 837 Shaw Road Date Received 03/05/03 <br />' S Client Contact Bill Little Date Extracted 03/05/03-03/11/03 <br /> tockton, CA 95215 <br /> Client P O Date Analyzed 03/05/03-03/11/03 <br />' Oxygenated Volatile Organics by P&T and GC/MS* <br /> F-uracnonMethod SW5030B Analytical Method SW8260B Work Order 0303039 <br />' Lab ID 0303039-OOIB 0303039-002B 10303039-003B 0303039-004B <br /> Client ID MW1/030403 MW2/030403 MW3/030403 MW4/030403 Repotting Limit for <br />' Matrix ----—W — W -------W---- ----- —W- --- DF=l <br /> DF 1 330 1 1 S W <br />' Compound Concentration ug/kg pg/L <br /> Dusopropyl ether(DIPE) ND ND<170 ND ND NA 05 <br />' Ethyl tert-butyl ether(ETRE) ND ND<170 ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 59 9200 31 ND NA 05 <br /> Cert-Amyl methyl ether(TAME) ND ND<170 ND ND NA 05 <br />' . t-Butyl alcohol(TBA) ND ND<1700 ND ND NA 50 <br /> Surrogate Recoveries(%) <br />' %SS 94 1 950 95 5 111 <br />' Comments <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported in lig/L,soiVsludge/solid samples in gg/kg, wipe samples in ltg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />