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Castle Analytical Laboratory, Atwater, CA <br /> ILab Report No H4062109 Date 06/30/2004 Page_9 <br /> Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW50305 <br />' Field ID MW-17 Lab Samp ID 7085-17W <br /> Descr/Location MW-17 Recd Date 06/22/2004 <br />' Sample Date 06/18/2004 Prep Date 06/27/2004 <br /> Sample Time 1900 Analysis Date 06/27/2004 <br /> Matrix Water QC Batch VWMS-6274 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Did <br /> Methyl-tent-butyl ether(MTBE) 289 50 MRL 130. UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L. 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DtPE) 0155 05 MRL ND UG/L 1 <br />' tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> 1,2-DEchloroethane 0 081 05 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63.132 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 59`135 SLSA 946% 1 <br /> Approved by I ��i Date <br />