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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H4062109 Date 06/30/2004 Page 10 <br />' Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-18 Lab Samp ID 7085-18W <br /> Descr/Location MW-18 Recd Date 06/22/2004 <br />' Sample Date 06/18/2004 Prep Date 06/27/2004 <br /> Sample Time 1509 Analysis Date 06/27/2004 <br /> Matrix Water QC Batch VWMS-6274 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br />' Methyl-tert-butyl ether(MTBE) 0 289 05 MRL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETRE) 0 084 05 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0155 06 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0 081 05 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UG/L 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 104% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 999% 1 <br /> I <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> i <br /> Approved by �i�/ Date <br /> 1 <br />