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North Coast Laboratories, Ltd. Date: 20-Sep-00 <br /> CLIENT: McCampbell Analytical QC SUMMARY REPORT <br /> Work Order: 0008530 <br /> Project: 2161 I/Home Depot.Tracy Sample Matrix Spike <br /> Sample ID 0008615-01AMS Batch ID: 2607 Test Code: 8140S Units: pg/g Analysis Date 9/15/00 10:13:04 PM Prep Date 8/31/00 <br /> Client ID: Run ID: ORGC10_000915A SegNo: 111174 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Hight-imit RPD Ref Val %RPD RPDLimit Qual <br /> Dichlorvos 1.065 0.50 1.25 0 85.2% 46 145 0 <br /> Mevinphos 2.468 1.0 2.50 0 98.7% 32 131 0 <br /> Ethoprophos 2.365 1.0 2.50 0.244 84.9% 38 135 0 <br /> Phorate 0.9088 0.50 1.25 0.260 51.9% 39 146 0 <br /> Demeton-S 4.139 2.0 5.00 1.34 56.0% 30 137 0 <br /> Diazinon 1.079 0.50 1.25 0 86.3% 42 132 0 <br /> Disulfoton 1.028 0.50 1.25 0 82.2% 37 139 0 <br /> Dimethoate 5.117 2.0 5.00 1.66 69.2% 17 134 0 <br /> Ronnel 1.092 0.50 1.25 0 87.3% 32 172 0 <br /> Methyl Parathion 1.006 0.50 1.25 0.175 66.5% 27 141 0 <br /> Chlorpyrifos 1.039 0.50 1.25 0 83.1% 37 150 0 <br /> Malathion 1.490 0.50 1.25 0.138 108% 48 139 0 <br /> Parathion 1.528 0.50 1.25 0 122% 28 152 0 <br /> Fenthion 1.189 0.50 1.25 0 95.1% 37 137 0 <br /> Tetrachlorvinphos 1.169 0.50 1.25 0 93.5% 44 135 0 <br /> Ethion 1.109 0.50 1.25 0.215 71.5% 51 128 0 <br /> Fensulfothion 2.586 1.0 2.50 0 103% 20 138 0 <br /> Azinphos 4.770 5.0 6.25 0 76.3% 38 146 0 J <br /> Coumaphos 5.863 2.5 6.25 1.27 73.5% 39 143 0 <br /> Triphenylphosphate 5.28 0.10 5.00 0 106% 30 137 0 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />