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CLIENT: McCantpbell Analytical QC SUMMARY REPORT <br /> Work Order: 0008530 <br /> Project: 21611/Horne Depot. Tracy Sample Matrix Spike Duplicate <br /> Sample ID 0008615-01AMSD Batch ID: 2607 Test Code: 8140S Units: pg/g Analysis Date 9/15/00 10:53:39 PM Prep Date 8/31/00 <br /> Client ID: Run ID: ORGC10_000915A SegNo: 111175 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] <br /> Dichlorvos 1.028 0.50 1.25 0 82.2% 46 145 1.06 3.52% 43 <br /> Mevinphos 2.181 1.0 2.50 0 87.2% 32 131 2.47 12.4% 35 <br /> Ethoprophos 1.917 1.0 2.50 0.244 66.9% 38 135 2.37 21.0% 25 <br /> Phorate 0.9981 0.50 1.25 0.260 59.0% 39 146 0.909 9.37% 34 <br /> Demeton-S 3.161 2.0 5.00 1.34 36.5% 30 137 4.14 26.8% 33 <br /> Diazinon 1.121 0.50 1.25 0 89.7% 42 132 1.08 3.79% 58 <br /> Disulfoton 1.020 0.50 1.25 0 81.6% 37 139 1.03 0.701% 33 <br /> Dimethoate 3 961 2.0 5.00 1.66 46.1% 17 134 5.12 25.5% 56 <br /> Ronnel 1070 0.50 1.25 0 85.6% 32 172 1.09 2.03% 30 <br /> Methyl Parathion 0.9683 0.50 1.25 0.175 63.5% 27 141 1.01 3.83% 37 <br /> Chlorpyrifos 1.040 0.50 1.25 0 83.2% 37 150 1.04 0.104% 34 <br /> Malathion 1486 0.50 1.25 0.138 108% 48 139 1.49 0.270% 36 <br /> Parathion 1.526 0.50 1.25 0 122% 28 152 1.53 0.140% 28 <br /> Fenthion 1.164 0.50 1.25 0 93.1% 37 137 1.19 2.12% 32 <br /> Tetrachlorvinphos 1.319 0.50 1.25 0 105% 44 135 1.17 12.0% 28 <br /> Ethion 0.6900 0.50 1.25 0.215 38.0% 51 128 1.11 46.5% 35 SR <br /> Fensulfothion 1.783 1.0 2.50 0 71.3% 20 138 2.59 36.7% 52 <br /> Azinphos 2.821 5.0 6.25 0 45.1% 38 146 4.77 0% 32 J <br /> Coumaphos 3.927 2.5 6.25 1.27 42.5% 39 143 5.86 39.5% 32 R <br /> Trip henylphosphate 5.32 0.10 5.00 0 106% 30 137 5.28 0.775% 31 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />