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04/25/2008 21 08 FAX 7077487717 (707)748-7717 Z012/014 <br /> 110 2nd AveoLLe Suuth.#1D7.Pacheco,CA 94M-1560 <br /> Trlephone 925-798.1620 Fax:923-798 ca 72 11 Com <br /> !� �, CCampbeil Analytie3l, 11aC. wrbsita:www.Racat+�belt.com t-m5il:muin(a�mc mPbe . <br /> QC SUMMARY REPORT FOR SW8260B <br /> W orlcOrd er: 0603377 <br /> QC Matrix; Water <br /> W.O.Sample Matrix: Water <br /> Extraction: PRVOCMS_W 8atchlD:20826 Spiked Sample ID: 0603377-001A <br /> EPA Method: SW82608 <br /> Spiked MS MSD MS-MSD LCS LCSD :LCS_LCSQ Acceptance Criteria <br /> Sample (°o <br /> Analyte rn - - 1%ROD °I°Ree. %Rec. %RPD MS I MSD LCS/LCSD <br /> pg/L Ng/L %Rec. %ReC. <br /> 2.61 70-130 70-130 <br /> 94.9 0.890 91.2 93.6 <br /> ND l0 95.8 ^ _ _ _ - - -- - - - - •- 70-130 <br /> .. <br /> tartAmyl methyl ether(TAME) -- - - - 1,28 115 116 <br /> U.376 70-130 - <br /> -- - - - - - ND 1p 117 116 = 70•i30 70-130 <br /> Benzene _ T p.691 101 106 5.34 _ <br /> -_ No SO 9G.5 97.2 i_ _ - - - - - - - __. -.- 70.130 <br /> t-Butyl alcohol(TBA) - _ - _ - - - - 91 93-y 2.98 70-130 <br /> - -. ND 10 94.9 98.1 - 3.31 _- - -- -- .- - -... 70,130 70-130 <br /> ChlorobtW-ne - - -- - - - 1.49 112 its 2.83 <br /> - - '- '- - ND 10 118 120 - - -. .- - - - -- - <br /> 1,2-Dibromoethane(EDO) _ - -• -. - - - - - 106 106 0 70-130 70-130 <br /> 2 No l0 114 114 n 70•130 <br /> 1.22 . <br /> 1,2-Diehloroethane(1,2-DCA)) - 807 81.2 0.685 70-130 _ <br /> _ ND 10 80.8 81.8 <br /> l,l-Dichloroethene _ _ _ - - - -t- -j 116 2.01 70,130 70-130 <br /> - - - - ND !0 119 117 1.79 114 - -- -- <br /> ND ether(DIPS) - -_ -. 105 0.562 70-130 70•130 <br /> NT) 10 log I 110 I.89 104. - -- - -- •-- - - -- <br /> i;tllyl tett-butyl ether(ETRE) - - - _-- - - - - 102 105 2.83 70-t30 70-130 <br /> - - NO 10 107 108 0.765 - - - -. - ..._ - <br /> Methyl-t-butyl ether(MTBE) N - -. -- T - - .- l 13 1 l6 2.77 70• 130 10-130 <br /> _ -. -- - - - ND 10 11.9 119 - 0 - -. .- - -- - ._.... _ _.. .... <br /> 'Poluene _ _ - - - -' - <br /> - --- - - - 10 94-3� 95.2 0.938 91.4 9z.1 0-788 70 130 70- 130 <br /> Trichloroethene NO 70-130 <br /> 106 10 102 102 0 103.T 1Ul- 2,07 7U-130 --- <br /> %SSI: -r-- p 70-130 70-110 <br /> -----= 10 gg <br /> 99 �98 _ 0 _ _ 98 98- -- - - -- - -- ._.. .... <br /> - -- - - - -- - 106 105 0.383 70-130 70,130 <br /> t0 106 106 0 <br /> %SS3: I]0 <br /> this ess e?ttrdctinn batch were ND lthan the method RL with the following <br /> All target compounds in the Method Blank of cxcCPtions: <br /> NONE <br /> C 0 Y <br /> Date Sampled Date SxtraCted Date Analyted <br /> Sample ID Date Sampled Date Extracted Date Analy2ed Sample ID- - -_ _ -_ - --• <br /> 3377 UOlA -3/19lOG 11;00 AM 3/22/OG 3/22106 2:48 PM 0603377-002A 3/19/06 12:30 PM - 3/22/06 3/22106 3:30 PM <br /> 060. - <br /> 0603377-0o3A 3119106 2:45 PM _3/22/06 3/22/06 4:11 PM <br /> eke Dupllcata;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD'Relative Percent De; soon. <br /> IV =Matrix Spike;MSD=Matrix OP <br /> ",Lr <br /> Recovery=100-(MS-Sample)I(Amount Spiked);RPD P 100-(M$- MSD)/((MS+MSD)/2). <br /> MS I MSD,pike recoveries and/or%RPO may fall outside of laboratorY acceptance criteria due to one or more of the following reasons:a)the sample is inhcmogenocs AND <br /> relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery- <br /> contains significant concentrations of analyte <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte Concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water melrlX or sample diluted due to high matrix or analyte content j <br /> Laborato extrdctlon solvents such as meth ene chlorlde and acetone mav occasional!y appear in the method blank at low levels. <br /> QA/QC Officer <br /> DHS Certification No. 1644 <br />