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04125/2006 21 :08 FAX 7077487717 (707)748-7717 Z013/014 <br /> 110 2nd Avcnu++80 raL ilD7,P°oluCo•CA 94553-5560 <br /> 925-798-1620 Fyr;92S-791-1623 <br /> T°lephon�' 1S_om <br /> �I)W-�Camp�beBAnalytical, Inc. Website:www.n_.amplxtl.cont F.ittail:tnaintutnxcatt>Qbc <br /> 4 <br /> QC SUMMARY REPORT FOR S`V8260B <br /> W orkOrder: 0603377 <br /> QC Matrix: Water <br /> w.0,Sample Matrix: Water S piked Sdmpls ID: 0603377-004A <br /> EPA Method: SW8260$ <br /> Extraction: PRVOCMS-W Bateh1D:20836 <br /> LCSD LCS-LCSD Acceptance Criteria(%) <br /> Sample Spiked MS MSD MS-MSD - - - -- <br /> Ta %RpD /°Rec. %Rea. %RPD MS I MSD LCS I LCSD <br /> Anatyte - - ° <br /> pg/L og/L %Rec- /°Rec. ; 70- 130 70- 130 <br /> 2.30 92.6 � 94,6 2.1_ <br /> ND 10 95.8 98.1 - - - -- -- - - - - --- - 70 130 <br /> Cert-Amyl methyl ether(TAME) - -_ - - - --- 117 'is 0.961 70-130 --- <br /> - - - - - 10 JIS - 119 1.18 -�.- <br /> - - - ND 2.92 70,130 70-130 <br /> Benzene = 1.05 99.5 102 - -- - - - -.. ... <br /> ND 50 97,8 98.9 - - - - - - -- - - - -- 70 130 <br /> t-Butyl alcohol(TBA) - - ----- -- 94.5 94.2 0.30.1 - 70_l30 -. -,_ -.. <br /> _ - - l0 93.3 97.8 4,69 _ _ -- - <br /> -- ND - 70-l30 70-130 <br /> Chlorobenzene -- - - --+ 116 u 118 1.09 - - - _ <br /> ------ 10 119 I 120 0.845 -- -.-- <br /> ND -}--, 0 - S.SG 10.130 70-130 <br /> 1,2 Dibromoethanc(fiUB) _-- - - - 107 113 _ <br /> ND to 114 114 = 70-130 <br /> 1,2,Dichloroethane(1,2-DCA) 80 3 84-4 4.93 70-130_ _ -- -- - <br /> - t0 80.4 80.7 0.430 - - - -- - - - - <br /> ND -- - - - -. - - 0 70.130 7t1- 130 <br /> 1,1-Dichlorocthene - - - - - - - r 1.52 118 118 ----- <br /> - - - -- - - - - ND 10 117 I t9 =- 70.130 <br /> Diisopropyl ether(DIPS)-- - J 105 109 <br /> ND 3,44 70_130 _ - - <br /> 10 l(19 112 2.46 _- - - -- <br /> 1 ether(FTBE) -- -- - - - - - 4.13 70-130 70-130 <br /> Ethyl tort-huty -_- - - - - p 108 109 0.830 104 - - -- - - - --. 1 <br /> - - - ND -- - - t.a2 70-t30 70-130 <br /> Methyl-t butyl ether(MTBE) _ -- -- - --- 2.46 1 l7 115 _ - --- - __ .- _,. .. <br /> - - - <br /> - - --- - l0 1iG i 119 s - -- - -- 94.4 --- -3.15 <br /> N 70-130 70-130 <br /> Toluene - -- - 95,8 L54 91.E <br /> - - - - - - -- D to 94.3 70- 130 , <br /> Trichlaroethenc lot 106 4.88 7o-130^-- <br /> 105 10 104 104 0 - -�- <br /> 70-130 70 130 <br /> 96 99 0.487 __ -- -- -- <br /> 99 98 10 98 -- - - - - -. -. .- <br /> %SS2: _ -- -- - - T 103 105 2.04 70 <br /> 112 1 U 130 70-l30 <br /> - - - 104 1 104 0 <br /> ._ --- - -- . <br /> %SS3: <br /> n batch were ND less than the method RL with the following exceptions' <br /> All target compuunds in the Method Blank of this extraCtio <br /> NONE <br /> T 3 M Y <br /> Date Sampled Date Extracted Date Analyzed <br /> Date Sampled Date Extracted Date Analyzed Sampl®ID <br /> Sample ID - <br /> OG(13377 004A - _3/19/06 4:20 PM -3122/06 3122106 4 56 PM - - - - - - <br /> MS=Matrix Splko;MSO=Matnx Spike Duplicate;LCS=Lenoratory Control SampW LCSD=Laboratory Control sample Duplicate;RPD=Ralath a Percent Deviation. <br /> %Recovery=100 (MS-Sample)I(Amount Spiked);RPD!100-(MS- MSD)I((MS+MSD)/2)- <br /> the <br /> amount Spiked,or b)the spiked sample's matrix Interferes with <br /> contains significant concentrations of analyte relative to the spike recovery. <br /> MS 1 MSD spike recoveries and!or may fall outside of laboratory acceptance criteria due to one or more of the falitnNing reasons:a)the sample is inhomogenous AN <br /> N/A=not enough Sample to perform matrix spike and matrix spike duplicate, <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for waterblank at for levels- <br /> Lebo <br /> ple diluted due to high matrix or analyte Conten, <br /> Leborato extraction solvents such as meth one chloride and acetone ma occaslonetl B ear in the method <br /> OQA/QC Officer <br /> DHS Certification No. 1644 <br />