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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Lab Control Spike/ Method: 8270C <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-22895 Preparation: 3550B <br /> LCS Lab Sample ID:LCS 720-22895/2-A Analysis Batch: 720-22967 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22895 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.13 g <br /> Date Analyzed: 06/21/2007 1127 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1847 Injection Volume: <br /> LCSD Lab Sample ID:LCSD 720-22895/3-A Analysis Batch: 720-22967 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22895 Lab File ID: c:\saturnws\epdata\data\200 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.29 g <br /> Date Analyzed: 06/21/2007 1156 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1847 Injection Volume: <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Naphthalene 76 73 21 - 133 5 35 <br /> Acenaphthene 73 71 40- 145 2 35 <br /> Acenaphthylene 77 77 33- 145 1 35 <br /> Fluorene 78 78 50- 121 0 35 <br /> Phenanthrene 75 77 10- 130 2 35 <br /> Anthracene 79 76 27- 133 4 35 <br /> Benzo[a]anthracene 83 84 33- 143 0 35 <br /> Chrysene 83 84 17- 168 1 35 <br /> Benzo[a]pyrene 83 79 17- 163 6 35 <br /> Benzo[b]fluoranthene 90 88 24- 159 2 35 <br /> Benzo[k]fluoranthene 80 79 11 - 162 2 35 <br /> Benzo[g,h,i]perylene 89 85 9-219 5 35 <br /> Indeno[1,2,3-cd]pyrene 93 92 9- 171 2 35 <br /> Fluoranthene 78 77 26- 137 2 35 <br /> Pyrene 80 81 52- 115 0 35 <br /> Dibenz(a,h)anthracene 97 96 9- 171 2 35 <br /> Surrogate LCS% Rec LCSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 78 79 30- 115 <br /> Terphenyl-d14 85 87 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 187 of 222 06/25/2007 <br />